Methyl 4-[2-(benzyloxy)-1-naphthyl]-3-[(ethoxycarbonyl)oxy]-5-ethylbenzoate

Base Information

Chemical Name:Methyl 4-[2-(benzyloxy)-1-naphthyl]-3-[(ethoxycarbonyl)oxy]-5-ethylbenzoate
CAS No.:198993-95-2
Molecular Formula:C₃₀H₂₈O₆
Molecular Weight:484.549
Hs Code.:

Synonyms:Methyl 4-[2-(benzyloxy)-1-naphthyl]-3-[(ethoxycarbonyl)oxy]-5-ethylbenzoate

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Chemical Property of Methyl 4-[2-(benzyloxy)-1-naphthyl]-3-[(ethoxycarbonyl)oxy]-5-ethylbenzoate

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Technology Process of Methyl 4-[2-(benzyloxy)-1-naphthyl]-3-[(ethoxycarbonyl)oxy]-5-ethylbenzoate

There total 5 articles about Methyl 4-[2-(benzyloxy)-1-naphthyl]-3-[(ethoxycarbonyl)oxy]-5-ethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 541-41-3
chloroformic acid ethyl ester

: 2-[2-[1-(2-Benzyloxy-naphthalen-1-yl)-meth-(E)-ylidene]-but-(E)-ylidene]-succinic acid 1-methyl ester

: 198993-95-2
Methyl 4-[2-(benzyloxy)-1-naphthyl]-3-[(ethoxycarbonyl)oxy]-5-ethylbenzoate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 0.5h; Ambient temperature;
DOI:10.1016/S0040-4020(97)01054-5

Reference yield:

: 52805-48-8
2-(Benzyloxy)-1-naphthaldehyde

: 198993-95-2
Methyl 4-[2-(benzyloxy)-1-naphthyl]-3-[(ethoxycarbonyl)oxy]-5-ethylbenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH / 1.) DME, mineral oil, room temperature, 1 h, 2.) DME, mineral oil, 50 deg C, 3 h

2: 96 percent / LiAlH₄ / diethyl ether

3: 76 percent / MnO₂ / CHCl₃

4: 69 percent / NaOMe / methanol / 0.5 h / 40 °C

5: 78 percent / Et₃N / tetrahydrofuran / 0.5 h / Ambient temperature

With manganese(IV) oxide; lithium aluminium tetrahydride; sodium methylate; sodium hydride; triethylamine; In tetrahydrofuran; methanol; diethyl ether; chloroform;
DOI:10.1016/S0040-4020(97)01054-5

Reference yield:

: 2-[1-(2-Benzyloxy-naphthalen-1-yl)-meth-(E)-ylidene]-butan-1-ol

: 198993-95-2
Methyl 4-[2-(benzyloxy)-1-naphthyl]-3-[(ethoxycarbonyl)oxy]-5-ethylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / MnO₂ / CHCl₃

2: 69 percent / NaOMe / methanol / 0.5 h / 40 °C

3: 78 percent / Et₃N / tetrahydrofuran / 0.5 h / Ambient temperature

With manganese(IV) oxide; sodium methylate; triethylamine; In tetrahydrofuran; methanol; chloroform;
DOI:10.1016/S0040-4020(97)01054-5