macrocycle (Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu

Base Information

Chemical Name:macrocycle (Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu
CAS No.:1321841-94-4
Molecular Formula:C₅₀H₆₉N₇O₉
Molecular Weight:912.139
Hs Code.:

Synonyms:macrocycle (Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu

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Chemical Property of macrocycle (Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu

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Technology Process of macrocycle (Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu

There total 5 articles about macrocycle (Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: HO-Phe-D-Phe-N-Me-Lys(Boc)-Leu-Lys(Cbz)-NH₂

: 1321841-94-4
macrocycle (Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu

Guidance literature:: With 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane;
DOI:10.1002/chem.201603464

Reference yield: 10.0%

: NH₂-(Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu-O-Resin

: 1321841-94-4
macrocycle (Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2011.09.096

Reference yield: 10.0%

: 1321841-92-2
NH₂-(Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu-OH

: 1321841-94-4
macrocycle (Boc)Lys-NMe-D-Phe-Phe-(Cbz)Lys-Leu

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.06.083