N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine

Base Information

Chemical Name:N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine
CAS No.:85923-42-8
Molecular Formula:C₂₂H₂₄N₂O₃S
Molecular Weight:396.51
Hs Code.:

Synonyms:N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine

Suppliers and Price of N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine

Chemical Property:

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Technology Process of N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine

There total 9 articles about N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 64035-64-9
Trimethylsilylmethyl trifluoromethanesulfonate

: 81816-19-5
N-<<(3-methoxybenzenesulfonyl)-1H-indol-3-yl>methylene>-4-pentenylamine

: 85923-42-8
N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine

: 81816-20-8
[1-[1-(4-Methoxy-benzenesulfonyl)-2-trimethylsilanylmethyl-1H-indol-3-yl]-meth-(E)-ylidene]-pent-4-enyl-amine

: 80664-26-2
N-<(4-methoxyphenyl)sulfonyl>-2-methylindole-3-carboxaldehyde

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; -78 deg C then room temp.;
DOI:10.1016/S0040-4020(01)93262-4

Reference yield:

: 81816-20-8
[1-[1-(4-Methoxy-benzenesulfonyl)-2-trimethylsilanylmethyl-1H-indol-3-yl]-meth-(E)-ylidene]-pent-4-enyl-amine

: 85923-42-8
N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine

Guidance literature:: With cesium fluoride; In various solvent(s); at 70 ℃; for 2h;
DOI:10.1016/S0040-4020(01)93262-4

Reference yield:

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 85923-42-8
N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride, 2.) imidazole / 1.) glyme, 20 deg C, 1.5 h, reflux, 15 min, 2.) 20 deg C, 15 h

2: 2.) Na₂SO₄ / 1.) benzene, 1 h, 2.) 2 h

With 1H-imidazole; sodium hydride; sodium sulfate;
DOI:10.1021/ja00352a037