N₂-cycloheptyl-N₄-(3-fluoro-4-methoxy-phenyl)-N₆-methyl-N₆-(1-methyl-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

Base Information

• Chemical Name: N₂-cycloheptyl-N₄-(3-fluoro-4-methoxy-phenyl)-N₆-methyl-N₆-(1-methyl-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine
• CAS No.: 502767-70-6
• Molecular Formula: C₂₄H₃₆FN₇O
• Molecular Weight: 457.595

Synonyms:N₂-cycloheptyl-N₄-(3-fluoro-4-methoxy-phenyl)-N₆-methyl-N₆-(1-methyl-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

Chemical Property of N₂-cycloheptyl-N₄-(3-fluoro-4-methoxy-phenyl)-N₆-methyl-N₆-(1-methyl-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of N₂-cycloheptyl-N₄-(3-fluoro-4-methoxy-phenyl)-N₆-methyl-N₆-(1-methyl-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

There total 4 articles about N₂-cycloheptyl-N₄-(3-fluoro-4-methoxy-phenyl)-N₆-methyl-N₆-(1-methyl-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

Methyl-(1-methyl-[4]piperidyl)-amin (73579-08-5) + 1,3,5-trichloro-2,4,6-triazine (108-77-0) + cycloheptanamine (5452-35-7) + 3-fluoro-4-methoxyaniline (366-99-4) → N2-cycloheptyl-N4-(3-fluoro-4-methoxy-phenyl)-N6-methyl-N6-piperidin-4-yl-1,3,5-triazine-2,4,6-triamine (502767-71-7) + N2-cycloheptyl-N4-(3-fluoro-4-methoxy-phenyl)-N6-methyl-N6-(1-methyl-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine (502767-70-6)

Guidance literature:

1,3,5-trichloro-2,4,6-triazine; 3-fluoro-4-methoxyaniline; With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; acetonitrile; at -20 - 20 ℃; for 2h;

cycloheptanamine; With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane-d8; acetonitrile; at 20 ℃;

Methyl-(1-methyl-[4]piperidyl)-amin; With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane-d8; acetonitrile; Heating / reflux;

Reference yield: 28.0%

1-ethyl-2-pyrrolidinemethanamine (26116-12-1) + 6-chloro-N2-cycloheptyl-N4-(3-fluoro-4-methoxy-phenyl)-[1,3,5]triazine-2,4-diamine (502767-47-7) → N2-cycloheptyl-N4-(3-fluoro-4-methoxy-phenyl)-N6-methyl-N6-piperidin-4-yl-1,3,5-triazine-2,4,6-triamine (502767-71-7) + N2-cycloheptyl-N4-(3-fluoro-4-methoxy-phenyl)-N6-methyl-N6-(1-methyl-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine (502767-70-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; acetonitrile; Heating / reflux;

Reference yield: 28.0%

Methyl-(1-methyl-[4]piperidyl)-amin (73579-08-5) + 6-chloro-N2-cycloheptyl-N4-(3-fluoro-4-methoxy-phenyl)-[1,3,5]triazine-2,4-diamine (502767-47-7) → N2-cycloheptyl-N4-(3-fluoro-4-methoxy-phenyl)-N6-methyl-N6-piperidin-4-yl-1,3,5-triazine-2,4,6-triamine (502767-71-7) + N2-cycloheptyl-N4-(3-fluoro-4-methoxy-phenyl)-N6-methyl-N6-(1-methyl-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine (502767-70-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile; Heating / reflux;

upstream raw materials:

1-ethyl-2-pyrrolidinemethanamine

6-chloro-N₂-cycloheptyl-N₄-(3-fluoro-4-methoxy-phenyl)-[1,3,5]triazine-2,4-diamine

Methyl-(1-methyl-[4]piperidyl)-amin

1,3,5-trichloro-2,4,6-triazine

Downstream raw materials:

N₂-cycloheptyl-N₄-(3-fluoro-4-methoxy-phenyl)-N₆-methyl-N₆-(1-methyl-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine; hydrogen chloride salt

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