N'-{4-[(tert-butyldimethylsilyl)oxy]cyclohexylidene}-4-methylbenzene-1-sulfonohydrazide

Base Information

Chemical Name:N'-{4-[(tert-butyldimethylsilyl)oxy]cyclohexylidene}-4-methylbenzene-1-sulfonohydrazide
CAS No.:569330-35-4
Molecular Formula:C₁₉H₃₂N₂O₃SSi
Molecular Weight:396.626
Hs Code.:

Synonyms:N'-{4-[(tert-butyldimethylsilyl)oxy]cyclohexylidene}-4-methylbenzene-1-sulfonohydrazide

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Chemical Property of N'-{4-[(tert-butyldimethylsilyl)oxy]cyclohexylidene}-4-methylbenzene-1-sulfonohydrazide

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Technology Process of N'-{4-[(tert-butyldimethylsilyl)oxy]cyclohexylidene}-4-methylbenzene-1-sulfonohydrazide

There total 4 articles about N'-{4-[(tert-butyldimethylsilyl)oxy]cyclohexylidene}-4-methylbenzene-1-sulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 55145-45-4
4-(tert-butyldimethylsilyloxy)cyclohexanone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 569330-35-4
N'-{4-[(tert-butyldimethylsilyl)oxy]cyclohexylidene}-4-methylbenzene-1-sulfonohydrazide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/ol0346685

Reference yield:

: 556-48-9
1,4-Cyclohexanediol

: 569330-35-4
N'-{4-[(tert-butyldimethylsilyl)oxy]cyclohexylidene}-4-methylbenzene-1-sulfonohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / imidazole / dimethylformamide; tetrahydrofuran / 0 °C

2: 98 percent / pyridinium chlorochromate / CH₂Cl₂ / 6 h / 20 °C

3: 98 percent / tetrahydrofuran / 2 h / 20 °C

With 1H-imidazole; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol0346685

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 569330-35-4
N'-{4-[(tert-butyldimethylsilyl)oxy]cyclohexylidene}-4-methylbenzene-1-sulfonohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / imidazole / dimethylformamide; tetrahydrofuran / 0 °C

2: 98 percent / pyridinium chlorochromate / CH₂Cl₂ / 6 h / 20 °C

3: 98 percent / tetrahydrofuran / 2 h / 20 °C

With 1H-imidazole; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol0346685