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5-(4-[3-(hexahydro-1H-azepin-1-yl)propoxy]phenyl)pentyl methanesulfonate

Base Information Edit
  • Chemical Name:5-(4-[3-(hexahydro-1H-azepin-1-yl)propoxy]phenyl)pentyl methanesulfonate
  • CAS No.:955360-14-2
  • Molecular Formula:C21H35NO4S
  • Molecular Weight:397.579
  • Hs Code.:
  • Mol file:955360-14-2.mol
5-(4-[3-(hexahydro-1H-azepin-1-yl)propoxy]phenyl)pentyl methanesulfonate

Synonyms:5-(4-[3-(hexahydro-1H-azepin-1-yl)propoxy]phenyl)pentyl methanesulfonate

Suppliers and Price of 5-(4-[3-(hexahydro-1H-azepin-1-yl)propoxy]phenyl)pentyl methanesulfonate
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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 5-(4-[3-(hexahydro-1H-azepin-1-yl)propoxy]phenyl)pentyl methanesulfonate Edit
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Technology Process of 5-(4-[3-(hexahydro-1H-azepin-1-yl)propoxy]phenyl)pentyl methanesulfonate

There total 4 articles about 5-(4-[3-(hexahydro-1H-azepin-1-yl)propoxy]phenyl)pentyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jm1013874
Guidance literature:
Multi-step reaction with 3 steps
1: di-tert-butyl-diazodicarboxylate; triphenylphosphine / tetrahydrofuran / -20 - 75 °C
2: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.27 h / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere
With lithium aluminium tetrahydride; di-tert-butyl-diazodicarboxylate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; 1: Mitsunobu reaction;
DOI:10.1021/jm1013874
Guidance literature:
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.27 h / Inert atmosphere
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere
With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm1013874
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