1,1,1,3,3,3-Hexamethyl-2-(2,4,6-triisopropyl-phenyl)-2-(2,4,6-trimethyl-phenyl)-trisilane

Base Information

• Chemical Name: 1,1,1,3,3,3-Hexamethyl-2-(2,4,6-triisopropyl-phenyl)-2-(2,4,6-trimethyl-phenyl)-trisilane
• CAS No.: 149209-42-7
• Molecular Formula: C₃₀H₅₂Si₃
• Molecular Weight: 496.999
• Mol file: 149209-42-7.mol

Synonyms:1,1,1,3,3,3-Hexamethyl-2-(2,4,6-triisopropyl-phenyl)-2-(2,4,6-trimethyl-phenyl)-trisilane

Chemical Property of 1,1,1,3,3,3-Hexamethyl-2-(2,4,6-triisopropyl-phenyl)-2-(2,4,6-trimethyl-phenyl)-trisilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1,1,1,3,3,3-Hexamethyl-2-(2,4,6-triisopropyl-phenyl)-2-(2,4,6-trimethyl-phenyl)-trisilane

There total 1 articles about 1,1,1,3,3,3-Hexamethyl-2-(2,4,6-triisopropyl-phenyl)-2-(2,4,6-trimethyl-phenyl)-trisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

chloro-trimethyl-silane (75-77-4) + Dichloro-(2,4,6-triisopropyl-phenyl)-(2,4,6-trimethyl-phenyl)-silane (107742-37-0) → 1,1,1,3,3,3-Hexamethyl-2-(2,4,6-triisopropyl-phenyl)-2-(2,4,6-trimethyl-phenyl)-trisilane (149209-42-7)

Guidance literature:

With lithium; In tetrahydrofuran; for 6h; Heating;

DOI:10.1016/0022-328X(93)80035-A

Reference yield: 43.0%

1,1,1,3,3,3-Hexamethyl-2-(2,4,6-triisopropyl-phenyl)-2-(2,4,6-trimethyl-phenyl)-trisilane (149209-42-7) + (all-R)-3-(Pyridin-2-yl)-2-azabicyclo[3.3.0]oct-2-ene (349558-29-8) → (3aR,11aR,RSSi)-1,2,3,3a,11,11a-hexahydro-5-(2,4,6-trimethylphenyl)-5-(2,4,6-triisopropylphenyl)cyclopenta[4',5']pyrrolo[1',2':3,4][1,3,2]diazasilolo[1,5-a]pyridine

Guidance literature:

In hexane; at 20 ℃; for 6h; Irradiation;

Reference yield:

1,1,1,3,3,3-Hexamethyl-2-(2,4,6-triisopropyl-phenyl)-2-(2,4,6-trimethyl-phenyl)-trisilane (149209-42-7) → C48H68Si2

Guidance literature:

In pentane; at -60 ℃; for 48h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Irradiation;

DOI:10.1016/0022-328X(93)80035-A

upstream raw materials:

chloro-trimethyl-silane

Dichloro-(2,4,6-triisopropyl-phenyl)-(2,4,6-trimethyl-phenyl)-silane