7,8-dihydro-2-(4-methoxyphenyl)-7,7-dimethyl-4-(3-nitrophenyl)quinolin-5(1H,4H,6H)-one

Base Information

• Chemical Name: 7,8-dihydro-2-(4-methoxyphenyl)-7,7-dimethyl-4-(3-nitrophenyl)quinolin-5(1H,4H,6H)-one
• CAS No.: 1446490-97-6
• Molecular Formula: C₂₄H₂₄N₂O₄
• Molecular Weight: 404.466

Synonyms:7,8-dihydro-2-(4-methoxyphenyl)-7,7-dimethyl-4-(3-nitrophenyl)quinolin-5(1H,4H,6H)-one

Chemical Property of 7,8-dihydro-2-(4-methoxyphenyl)-7,7-dimethyl-4-(3-nitrophenyl)quinolin-5(1H,4H,6H)-one

Chemical Property:

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Technology Process of 7,8-dihydro-2-(4-methoxyphenyl)-7,7-dimethyl-4-(3-nitrophenyl)quinolin-5(1H,4H,6H)-one

There total 5 articles about 7,8-dihydro-2-(4-methoxyphenyl)-7,7-dimethyl-4-(3-nitrophenyl)quinolin-5(1H,4H,6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-nitro-benzaldehyde (99-61-6) + dimedone (126-81-8) + 1-(4-methoxyphenyl)ethanone (100-06-1) → 7,8-dihydro-2-(4-methoxyphenyl)-7,7-dimethyl-4-(3-nitrophenyl)quinolin-5(1H,4H,6H)-one (1446490-97-6)

Guidance literature:

With ammonium carbonate; In water; at 20 ℃; Green chemistry;

DOI:10.1039/c3gc40441b

Reference yield:

1-(4-methoxyphenyl)-3-(3-nitrophenyl)prop-2-en-1-one (68063-55-8) + 1-amino-5,5-dimethylcyclohexen-3-one (873-95-0) → 7,8-dihydro-2-(4-methoxyphenyl)-7,7-dimethyl-4-(3-nitrophenyl)quinolin-5(1H,4H,6H)-one (1446490-97-6)

Guidance literature:

With mesoporous silica MCM-41-supported hexafluorophosphoric acid; In water; at 20 ℃; Green chemistry;

DOI:10.1039/c3gc40441b

Reference yield:

3-nitro-benzaldehyde (99-61-6) + dimedone (126-81-8) + 1-(4-methoxyphenyl)ethanone (100-06-1) → 1-(4-methoxyphenyl)-3-(3-nitrophenyl)prop-2-en-1-one (68063-55-8) + 7,8-dihydro-2-(4-methoxyphenyl)-7,7-dimethyl-4-(3-nitrophenyl)quinolin-5(1H,4H,6H)-one (1446490-97-6) + 1-amino-5,5-dimethylcyclohexen-3-one (873-95-0)

Guidance literature:

With ammonium carbonate; In water; at 20 ℃; for 1h; Green chemistry;

DOI:10.1039/c3gc40441b

upstream raw materials:

dimedone

3-nitro-benzaldehyde

1-(4-methoxyphenyl)ethanone

1-(4-methoxyphenyl)-3-(3-nitrophenyl)prop-2-en-1-one

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