2,4,6-trichlorophenyl pyrimidine-5-carboxylate

Base Information

Chemical Name:2,4,6-trichlorophenyl pyrimidine-5-carboxylate
CAS No.:1402012-72-9
Molecular Formula:C₁₁H₅Cl₃N₂O₂
Molecular Weight:303.532
Hs Code.:

Synonyms:2,4,6-trichlorophenyl pyrimidine-5-carboxylate

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Chemical Property of 2,4,6-trichlorophenyl pyrimidine-5-carboxylate

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Technology Process of 2,4,6-trichlorophenyl pyrimidine-5-carboxylate

There total 2 articles about 2,4,6-trichlorophenyl pyrimidine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 4595-59-9
5-bromopyrimidine

: 4525-65-9
(2,4,6-trichlorophenyl) formate

: 1402012-72-9
2,4,6-trichlorophenyl pyrimidine-5-carboxylate

Guidance literature:: 5-bromopyrimidine; With tributyl-amine; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 100 ℃; Inert atmosphere;

(2,4,6-trichlorophenyl) formate; In toluene; at 100 ℃; Inert atmosphere;
DOI:10.1021/ol302593z

Reference yield:

: 88-06-2,67471-29-8
2,4,6-Trichlorophenol

: 1402012-72-9
2,4,6-trichlorophenyl pyrimidine-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 1 h / 20 - 60 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tributyl-amine / toluene / 100 °C / Inert atmosphere

2.2: 100 °C / Inert atmosphere

With tributyl-amine; palladium diacetate; acetic anhydride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene;
DOI:10.1021/ol302593z