Formic acid 6-(3,4-dimethoxy-phenyl)-1,6-dimethyl-7-oxo-azepan-4-yl ester

Base Information

Chemical Name:Formic acid 6-(3,4-dimethoxy-phenyl)-1,6-dimethyl-7-oxo-azepan-4-yl ester
CAS No.:97611-52-4
Molecular Formula:C₁₇H₂₃NO₅
Molecular Weight:321.373
Hs Code.:

Synonyms:Formic acid 6-(3,4-dimethoxy-phenyl)-1,6-dimethyl-7-oxo-azepan-4-yl ester

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Chemical Property of Formic acid 6-(3,4-dimethoxy-phenyl)-1,6-dimethyl-7-oxo-azepan-4-yl ester

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Technology Process of Formic acid 6-(3,4-dimethoxy-phenyl)-1,6-dimethyl-7-oxo-azepan-4-yl ester

There total 5 articles about Formic acid 6-(3,4-dimethoxy-phenyl)-1,6-dimethyl-7-oxo-azepan-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 97611-79-5
2-(3,4-Dimethoxy-phenyl)-2-methyl-pent-4-enoic acid methylamide

: 97611-52-4
Formic acid 6-(3,4-dimethoxy-phenyl)-1,6-dimethyl-7-oxo-azepan-4-yl ester

Guidance literature:: In formic acid; at 60 - 70 ℃; for 6h;
DOI:10.1248/cpb.33.340

Reference yield:

: 29207-02-1
methyl 2-(3,4-dimethoxyphenyl)propanoate

: 97611-52-4
Formic acid 6-(3,4-dimethoxy-phenyl)-1,6-dimethyl-7-oxo-azepan-4-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1) LDA / 1) THF, -78 deg C, 0.5 h

2: 10percent NaOH / ethanol / 2 h / Heating

3: SOCl₂ / benzene / 6 h / Heating

4: Na₂CO₃ / benzene / 0.08 h / 0 - 5 °C

5: 78 percent / formic acid / 6 h / 60 - 70 °C

With sodium hydroxide; thionyl chloride; sodium carbonate; lithium diisopropyl amide; In formic acid; ethanol; benzene;
DOI:10.1248/cpb.33.340

Reference yield:

: 2-(3,4-Dimethoxy-phenyl)-2-methyl-pent-4-enoyl chloride

: 97611-52-4
Formic acid 6-(3,4-dimethoxy-phenyl)-1,6-dimethyl-7-oxo-azepan-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂CO₃ / benzene / 0.08 h / 0 - 5 °C

2: 78 percent / formic acid / 6 h / 60 - 70 °C

With sodium carbonate; In formic acid; benzene;
DOI:10.1248/cpb.33.340