(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (R)-3-phenyl-2-allyl-2-cyanopropanoate

Base Information

Chemical Name:(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (R)-3-phenyl-2-allyl-2-cyanopropanoate
CAS No.:143100-10-1
Molecular Formula:C₃₅H₅₀N₂O₄S
Molecular Weight:594.859
Hs Code.:

Synonyms:(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (R)-3-phenyl-2-allyl-2-cyanopropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (R)-3-phenyl-2-allyl-2-cyanopropanoate

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Technology Process of (1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (R)-3-phenyl-2-allyl-2-cyanopropanoate

There total 3 articles about (1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (R)-3-phenyl-2-allyl-2-cyanopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 188183-31-5
(2RS)-(1S,2R,4R)-10-(Dicyclohexylsulfamoyl)isobornyl 3-phenyl-2-cyanopropanoate

: 106-95-6
allyl bromide

: 143100-10-1
(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (R)-3-phenyl-2-allyl-2-cyanopropanoate

Guidance literature:: With potassium carbonate; In acetone; for 24h; Ambient temperature;
DOI:10.1016/S0957-4166(96)00516-2

Reference yield:

: 188183-31-5
(2RS)-(1S,2R,4R)-10-(Dicyclohexylsulfamoyl)isobornyl 3-phenyl-2-cyanopropanoate

: 106-95-6
allyl bromide

: 143100-10-1
(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (R)-3-phenyl-2-allyl-2-cyanopropanoate

: 143100-11-2
(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (S)-3-phenyl-2-allyl-2-cyanopropanoate

Guidance literature:: With lithium diisopropyl amide; Yield given. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, -78 deg C, 1 h, 2.) THF, HMPA, -78 deg C to r.t.; r.t., 1 d;
DOI:10.1021/jo00088a034

Reference yield:

: 132640-95-0
(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (E)-2-cyanocinnamate

: 106-95-6
allyl bromide

: 143100-10-1
(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (R)-3-phenyl-2-allyl-2-cyanopropanoate

: 143100-11-2
(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (S)-3-phenyl-2-allyl-2-cyanopropanoate

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; L-Selectride; Yield given. Multistep reaction. Yields of byproduct given; 1.) ether, THF, 2 h, 2.) ether, THF, RT, 3 d;
DOI:10.1246/bcsj.65.1657