dimethyl 5-(N,N-dimethyl)aminoisophthalate

Base Information

Chemical Name:dimethyl 5-(N,N-dimethyl)aminoisophthalate
CAS No.:1301599-45-0
Molecular Formula:C₁₃H₁₇NO₄
Molecular Weight:251.282
Hs Code.:

Synonyms:dimethyl 5-(N,N-dimethyl)aminoisophthalate

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Chemical Property of dimethyl 5-(N,N-dimethyl)aminoisophthalate

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Technology Process of dimethyl 5-(N,N-dimethyl)aminoisophthalate

There total 1 articles about dimethyl 5-(N,N-dimethyl)aminoisophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 42268-88-2
1,3-dimethyl 5-(bromomethyl)benzene-1,3-dicarboxylate

: 124-40-3
dimethyl amine

: 1301599-45-0
dimethyl 5-(N,N-dimethyl)aminoisophthalate

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.3390/molecules181011938

Reference yield: 38.0%

: 1301599-45-0
dimethyl 5-(N,N-dimethyl)aminoisophthalate

: 1301599-47-2
(5-((dimethylamino)methyl)-1,3-phenylene)dimethanol

Guidance literature:: With lithium borohydride; ethanol; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.3390/molecules181011938

Reference yield:

: 1301599-45-0
dimethyl 5-(N,N-dimethyl)aminoisophthalate

: 1301599-51-8
1,3-bis(aminomethyl)-5-(N,N-dimethylamino)methylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: lithium borohydride; ethanol / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: diphenylphosphoranyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: water / tetrahydrofuran / 20 °C / Inert atmosphere

With lithium borohydride; ethanol; diphenylphosphoranyl azide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.3390/molecules181011938