1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethyl [4-(propan-2-yl)phenyl]carbamate

Base Information

Chemical Name:1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethyl [4-(propan-2-yl)phenyl]carbamate
CAS No.:1363792-18-0
Molecular Formula:C₂₁H₂₂FN₃O₂
Molecular Weight:367.423
Hs Code.:

Synonyms:1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethyl [4-(propan-2-yl)phenyl]carbamate

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Chemical Property of 1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethyl [4-(propan-2-yl)phenyl]carbamate

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Technology Process of 1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethyl [4-(propan-2-yl)phenyl]carbamate

There total 3 articles about 1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethyl [4-(propan-2-yl)phenyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 31027-31-3
4-isopropylphenylisocyanate

: 24155-46-2
1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol

: 1363792-18-0
1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethyl [4-(propan-2-yl)phenyl]carbamate

Guidance literature:: 1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol; With sodium hydride; In acetonitrile; at 20 ℃; for 2h;

4-isopropylphenylisocyanate; In acetonitrile; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2012.01.034

Reference yield:

: 24155-33-7
1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethanone

: 1363792-18-0
1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethyl [4-(propan-2-yl)phenyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / methanol

2.1: sodium hydride / acetonitrile / 2 h / 20 °C

2.2: 24 h / 20 °C

With sodium tetrahydroborate; sodium hydride; In methanol; acetonitrile;
DOI:10.1016/j.ejmech.2012.01.034

Reference yield:

: 403-29-2
2-bromo-4'-fluoroacetophenone

: 1363792-18-0
1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethyl [4-(propan-2-yl)phenyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide

2.1: sodium tetrahydroborate / methanol

3.1: sodium hydride / acetonitrile / 2 h / 20 °C

3.2: 24 h / 20 °C

With sodium tetrahydroborate; sodium hydride; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.ejmech.2012.01.034