2-{4-methoxy-3-[(3R)-tetrahydrofuranyloxy]phenyl}-5,5-dimethyl-[1,3,2]dioxaborinane

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Chemical Name:2-{4-methoxy-3-[(3R)-tetrahydrofuranyloxy]phenyl}-5,5-dimethyl-[1,3,2]dioxaborinane
CAS No.:784189-97-5
Molecular Formula:C₁₆H₂₃BO₅
Molecular Weight:306.167
Hs Code.:

Synonyms:2-{4-methoxy-3-[(3R)-tetrahydrofuranyloxy]phenyl}-5,5-dimethyl-[1,3,2]dioxaborinane

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Chemical Property of 2-{4-methoxy-3-[(3R)-tetrahydrofuranyloxy]phenyl}-5,5-dimethyl-[1,3,2]dioxaborinane

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Technology Process of 2-{4-methoxy-3-[(3R)-tetrahydrofuranyloxy]phenyl}-5,5-dimethyl-[1,3,2]dioxaborinane

There total 2 articles about 2-{4-methoxy-3-[(3R)-tetrahydrofuranyloxy]phenyl}-5,5-dimethyl-[1,3,2]dioxaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 784189-97-5
2-{4-methoxy-3-[(3R)-tetrahydrofuranyloxy]phenyl}-5,5-dimethyl-[1,3,2]dioxaborinane

Guidance literature:: (R)-(-)-3-(5-bromo-2-methoxyphenoxy)tetrahydrofuran; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1.5h;

With Trimethyl borate; In tetrahydrofuran; at 20 ℃;

2,2-Dimethyl-1,3-propanediol; In toluene; for 4h; Heating / reflux;

Reference yield: 35.0%

: 784189-99-7
(R)-(-)-3-(5-bromo-2-methoxyphenoxy)tetrahydrofuran

: 121-43-7,63156-11-6
Trimethyl borate

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 784189-97-5
2-{4-methoxy-3-[(3R)-tetrahydrofuranyloxy]phenyl}-5,5-dimethyl-[1,3,2]dioxaborinane

Guidance literature:: (R)-(-)-3-(5-bromo-2-methoxyphenoxy)tetrahydrofuran; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1.5h;

Trimethyl borate; In tetrahydrofuran; at -78 - 20 ℃;

2,2-Dimethyl-1,3-propanediol; In toluene; for 4h; Heating / reflux;

Reference yield: 79.0%

: 784189-98-6
5-bromo-1-(3,4-difluorobenzyl)-1H-pyrazole

: 784189-97-5
2-{4-methoxy-3-[(3R)-tetrahydrofuranyloxy]phenyl}-5,5-dimethyl-[1,3,2]dioxaborinane

: 1-(3,4-difluorobenzyl)-5-[4-methoxy-3-[(3R)-tetrahydrofuranyloxy]phenyl]-1H-pyrazole

Guidance literature:: With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride; In 1,2-dimethoxyethane; ethanol; water; at 140 ℃; for 0.0416667h;