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Technology Process of (CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(1+)*Cl(1-)=(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(Cl)

(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(1+)*Cl(1-)=(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(Cl)

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  • Chemical Name:(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(1+)*Cl(1-)=(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(Cl)
  • CAS No.:1106739-96-1
  • Molecular Formula:C19H26Cl3N2Ti*Cl
  • Molecular Weight:472.121
  • Hs Code.:
(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>NH<sub>2</sub>(CH<sub>2</sub>)3NC<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2TiCl<sub>3</sub><sup>(1+)</sup>*Cl<sup>(1-)</sup>=(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>NH<sub>2</sub>(CH<sub>2</sub>)3NC<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2TiCl<sub>3</sub>(Cl)

Synonyms:(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(1+)*Cl(1-)=(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(Cl)

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Chemical Property of (CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(1+)*Cl(1-)=(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(Cl)
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Technology Process of (CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(1+)*Cl(1-)=(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(Cl)

There total 1 articles about (CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(1+)*Cl(1-)=(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(Cl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1,3-bis(2,6-dimethylanilino)propane
72991-64-1

1,3-bis(2,6-dimethylanilino)propane

titanium tetrachloride
7550-45-0

titanium tetrachloride

(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>NH<sub>2</sub>(CH<sub>2</sub>)3NC<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2TiCl<sub>3</sub><sup>(1+)</sup>*Cl<sup>(1-)</sup>=(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>NH<sub>2</sub>(CH<sub>2</sub>)3NC<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2TiCl<sub>3</sub>(Cl)
1106739-96-1

(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(1+)*Cl(1-)=(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(Cl)

Guidance literature:
In toluene; (Ar); to soln. of TiCl4 in toluene was added at -20°C soln. of 1,3-(bis(2,6-dimethylanolino)propane in toluene; filtered, washed with pentane, elem. anal.;
DOI:10.1016/j.ica.2008.02.034

Reference yield: 99.0%

(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>NH<sub>2</sub>(CH<sub>2</sub>)3NC<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2TiCl<sub>3</sub><sup>(1+)</sup>*Cl<sup>(1-)</sup>=(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>NH<sub>2</sub>(CH<sub>2</sub>)3NC<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2TiCl<sub>3</sub>(Cl)
1106739-96-1

(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(1+)*Cl(1-)=(CH3)2C6H3NH2(CH2)3NC6H3(CH3)2TiCl3(Cl)

[Ti(1,3-bis(2,6-dimethylanilino)propane)Cl<sub>2</sub>]
179612-34-1

[Ti(1,3-bis(2,6-dimethylanilino)propane)Cl2]

Guidance literature:
With (C2H5)3N; In not given; byproducts: (C2H5)3N*HCl; excess of Et3N; yield detected by NMR;
DOI:10.1016/j.ica.2008.02.034
upstream raw materials:

1,3-bis(2,6-dimethylanilino)propane

titanium tetrachloride

Downstream raw materials:

[Ti(1,3-bis(2,6-dimethylanilino)propane)Cl2]

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