tert-butyl 3-(1-(4-bromo-1H-indole-2-carbonyl)piperidin-4-yl)benzylcarbamate

Base Information

Chemical Name:tert-butyl 3-(1-(4-bromo-1H-indole-2-carbonyl)piperidin-4-yl)benzylcarbamate
CAS No.:1411992-69-2
Molecular Formula:C₂₆H₃₀BrN₃O₃
Molecular Weight:512.447
Hs Code.:

Synonyms:tert-butyl 3-(1-(4-bromo-1H-indole-2-carbonyl)piperidin-4-yl)benzylcarbamate

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Chemical Property of tert-butyl 3-(1-(4-bromo-1H-indole-2-carbonyl)piperidin-4-yl)benzylcarbamate

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Technology Process of tert-butyl 3-(1-(4-bromo-1H-indole-2-carbonyl)piperidin-4-yl)benzylcarbamate

There total 1 articles about tert-butyl 3-(1-(4-bromo-1H-indole-2-carbonyl)piperidin-4-yl)benzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 16732-64-2
4-bromo-1H-indole-2-carboxylic acid

: 725228-49-9
tert-butyl 3-(piperidin-4-yl)benzylcarbamate

: 1411992-69-2
tert-butyl 3-(1-(4-bromo-1H-indole-2-carbonyl)piperidin-4-yl)benzylcarbamate

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

Reference yield:

: 1411992-69-2
tert-butyl 3-(1-(4-bromo-1H-indole-2-carbonyl)piperidin-4-yl)benzylcarbamate

: 73183-34-3
bis(pinacol)diborane

: 1411992-72-7
C₃₂H₄₂BN₃O₅

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; for 12h; Reflux;

Reference yield:

: 1411992-69-2
tert-butyl 3-(1-(4-bromo-1H-indole-2-carbonyl)piperidin-4-yl)benzylcarbamate

: 1411994-03-0
C₂₇H₃₄BN₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 12 h / Reflux

2: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; trifluoroacetic acid; In 1,4-dioxane; dichloromethane;