Nonanedioic acid 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester methyl ester

Base Information

Chemical Name:Nonanedioic acid 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester methyl ester
CAS No.:218899-23-1
Molecular Formula:C₂₇H₃₄O₈
Molecular Weight:486.562
Hs Code.:

Synonyms:Nonanedioic acid 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester methyl ester

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Chemical Property of Nonanedioic acid 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester methyl ester

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Technology Process of Nonanedioic acid 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester methyl ester

There total 3 articles about Nonanedioic acid 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 39604-68-7
2'-hydroxy-4',6-dimethoxy-2-(p-methoxyphenyl)acetophenone

: 56555-02-3
methyl 9-chloro-9-oxononanoate

: 218899-23-1
Nonanedioic acid 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester methyl ester

Guidance literature:: With pyridine; for 48h; Ambient temperature;
DOI:10.1055/s-1998-2221

Reference yield:

: 123-99-9,26776-28-3
azelaic acid

: 218899-23-1
Nonanedioic acid 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / Dowex 50W-X₂ / petroleum ether / 4 h / Heating

2: 81 percent / oxalyl chloride / 2 h / Heating

3: 62 percent / pyridine / 48 h / Ambient temperature

With pyridine; oxalyl dichloride; DOWEX 50W-X₂; In Petroleum ether;
DOI:10.1055/s-1998-2221

Reference yield:

: 2104-19-0
azelaic monomethyl ester

: 218899-23-1
Nonanedioic acid 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / oxalyl chloride / 2 h / Heating

2: 62 percent / pyridine / 48 h / Ambient temperature

With pyridine; oxalyl dichloride;
DOI:10.1055/s-1998-2221