3-methyl-3-(4-trimethylsilanyl-but-3-ynyl)-1-trimethylsilanyloxy-cyclohexene

Base Information

• Chemical Name: 3-methyl-3-(4-trimethylsilanyl-but-3-ynyl)-1-trimethylsilanyloxy-cyclohexene
• CAS No.: 886752-34-7
• Molecular Formula: C₁₇H₃₂OSi₂
• Molecular Weight: 308.611

Synonyms:3-methyl-3-(4-trimethylsilanyl-but-3-ynyl)-1-trimethylsilanyloxy-cyclohexene

Chemical Property of 3-methyl-3-(4-trimethylsilanyl-but-3-ynyl)-1-trimethylsilanyloxy-cyclohexene

Chemical Property:

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Technology Process of 3-methyl-3-(4-trimethylsilanyl-but-3-ynyl)-1-trimethylsilanyloxy-cyclohexene

There total 2 articles about 3-methyl-3-(4-trimethylsilanyl-but-3-ynyl)-1-trimethylsilanyloxy-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro-trimethyl-silane (75-77-4) + 3-methylcyclohexen-2-one (1193-18-6) + 1-chloro-5-trimethylsilyl-4-pentyne (58435-00-0) → 3-methyl-3-(4-trimethylsilanyl-but-3-ynyl)-1-trimethylsilanyloxy-cyclohexene (886752-34-7)

Guidance literature:

1-chloro-5-trimethylsilyl-4-pentyne; With magnesium; ethylene dibromide; In tetrahydrofuran; at -78 ℃; Reflux; Inert atmosphere;

With copper(l) iodide; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

chloro-trimethyl-silane; 3-methylcyclohexen-2-one; Further stages;

DOI:10.1021/jo802672t

Reference yield:

chloro-trimethyl-silane (75-77-4) + 3-methylcyclohexen-2-one (1193-18-6) + [4-(trimethylsilyl)but-3-ynyl]magnesium bromide (67781-10-6) → 3-methyl-3-(4-trimethylsilanyl-but-3-ynyl)-1-trimethylsilanyloxy-cyclohexene (886752-34-7)

Guidance literature:

[4-(trimethylsilyl)but-3-ynyl]magnesium bromide; With copper(l) iodide; In tetrahydrofuran; at -78 ℃; for 0.5h;

chloro-trimethyl-silane; 3-methylcyclohexen-2-one; With triethylamine; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1080/00397910903219484

Reference yield: 83.0%

3-methyl-3-(4-trimethylsilanyl-but-3-ynyl)-1-trimethylsilanyloxy-cyclohexene (886752-34-7) → 2-bromo-3-methyl-3-(4-trimethylsilyl-3-butynyl)-1-cyclohexanone (1239373-73-9)

Guidance literature:

With iron(III) chloride; sodium bromide; In acetonitrile; at 0 - 20 ℃;

DOI:10.1080/00397910903219484

upstream raw materials:

chloro-trimethyl-silane

3-methylcyclohexen-2-one

1-chloro-5-trimethylsilyl-4-pentyne

[4-(trimethylsilyl)but-3-ynyl]magnesium bromide

Downstream raw materials:

2-iodo-3-methyl-3-[4-(trimethylsilyl)-3-butynyl]-1-cyclohexanone

2-bromo-3-methyl-3-(4-trimethylsilyl-3-butynyl)-1-cyclohexanone

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