thiopropionic acid S-[3-(4-methoxyphenyl)-4,5-dihydro-isoxazol-5-ylmethyl]ester

Base Information

Chemical Name:thiopropionic acid S-[3-(4-methoxyphenyl)-4,5-dihydro-isoxazol-5-ylmethyl]ester
CAS No.:473253-52-0
Molecular Formula:C₁₄H₁₇NO₃S
Molecular Weight:279.36
Hs Code.:

Synonyms:thiopropionic acid S-[3-(4-methoxyphenyl)-4,5-dihydro-isoxazol-5-ylmethyl]ester

Suppliers and Price of thiopropionic acid S-[3-(4-methoxyphenyl)-4,5-dihydro-isoxazol-5-ylmethyl]ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of thiopropionic acid S-[3-(4-methoxyphenyl)-4,5-dihydro-isoxazol-5-ylmethyl]ester

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Technology Process of thiopropionic acid S-[3-(4-methoxyphenyl)-4,5-dihydro-isoxazol-5-ylmethyl]ester

There total 3 articles about thiopropionic acid S-[3-(4-methoxyphenyl)-4,5-dihydro-isoxazol-5-ylmethyl]ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 41820-22-8
allyl thiopropionate

: 74903-79-0
N-hydroxy-4-methoxybenzenecarboximidoyl chloride

: 473253-52-0
thiopropionic acid S-[3-(4-methoxyphenyl)-4,5-dihydro-isoxazol-5-ylmethyl]ester

Guidance literature:: With triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020183v

Reference yield:

: 70286-37-2
4-methoxy-benzaldehyde-(O-methyl-seqtrans-oxime )

: 473253-52-0
thiopropionic acid S-[3-(4-methoxyphenyl)-4,5-dihydro-isoxazol-5-ylmethyl]ester

Guidance literature:: Multi-step reaction with 2 steps

1: 11.1 g / N-chlorosuccinimide; HCl / dimethylformamide / 1 h / 20 °C

2: 64 percent / Et₃N / CH₂Cl₂; dimethylformamide

With hydrogenchloride; N-chloro-succinimide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020183v

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 473253-52-0
thiopropionic acid S-[3-(4-methoxyphenyl)-4,5-dihydro-isoxazol-5-ylmethyl]ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; aq. triethylamine / tetrahydrofuran / 4 h

2: 11.1 g / N-chlorosuccinimide; HCl / dimethylformamide / 1 h / 20 °C

3: 64 percent / Et₃N / CH₂Cl₂; dimethylformamide

With hydrogenchloride; N-chloro-succinimide; hydroxylamine hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020183v