(5,7-Bis-benzyloxy-4,6-dimethyl-1H-indol-3-ylmethyl)-trimethyl-ammonium; iodide

Base Information

Chemical Name:(5,7-Bis-benzyloxy-4,6-dimethyl-1H-indol-3-ylmethyl)-trimethyl-ammonium; iodide
CAS No.:99053-80-2
Molecular Formula:C₂₈H₃₃N₂O₂*I
Molecular Weight:556.487
Hs Code.:

Synonyms:(5,7-Bis-benzyloxy-4,6-dimethyl-1H-indol-3-ylmethyl)-trimethyl-ammonium; iodide

Suppliers and Price of (5,7-Bis-benzyloxy-4,6-dimethyl-1H-indol-3-ylmethyl)-trimethyl-ammonium; iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5,7-Bis-benzyloxy-4,6-dimethyl-1H-indol-3-ylmethyl)-trimethyl-ammonium; iodide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of (5,7-Bis-benzyloxy-4,6-dimethyl-1H-indol-3-ylmethyl)-trimethyl-ammonium; iodide

There total 12 articles about (5,7-Bis-benzyloxy-4,6-dimethyl-1H-indol-3-ylmethyl)-trimethyl-ammonium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7149-92-0
2,4-dimethoxy-3-methylbenzaldehyde

: 99053-80-2
(5,7-Bis-benzyloxy-4,6-dimethyl-1H-indol-3-ylmethyl)-trimethyl-ammonium; iodide

Guidance literature:: Multi-step reaction with 11 steps

1: 89 percent / KOH, NaBH₃CN / methanol / 2.5 h / 25 °C

2: 96 percent / CH₂Cl₂ / 3 h / 25 °C

3: 94 percent / Na, Fe(NO₃)*9H₂O / liquid ammonia / 4 h

4: 58 percent / NBS / benzene / 20 h / 25 °C

5: 86 percent / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 2 h; 2.) 25 deg C, 2 h

6: 78 percent / K₂CO₃, NaI / acetone / 5 h / Heating

7: 77 percent / NH₄OAc / acetic acid / 1.5 h / Heating

8: 48 percent / Cu(NO₃)2*3H₂O / acetic anhydride / 1 h / 65 °C

9: 92 percent / Fe, AcOH, silica gel / toluene / 1 h / Heating

10: H₂O; ethanol; acetic acid / 8 h / 25 °C

11: ethanol; ethyl acetate / 12 h

With potassium hydroxide; N-Bromosuccinimide; Fe(NO₃)*9H₂O; ammonium acetate; sodium; silica gel; boron tribromide; iron; sodium cyanoborohydride; potassium carbonate; copper(II) nitrate; acetic acid; sodium iodide; In methanol; ethanol; dichloromethane; ammonia; water; acetic anhydride; acetic acid; ethyl acetate; acetone; toluene; benzene;
DOI:10.1021/ja00311a065

Reference yield:

: 5673-07-4
2,6-dimethoxytoluene

: 99053-80-2
(5,7-Bis-benzyloxy-4,6-dimethyl-1H-indol-3-ylmethyl)-trimethyl-ammonium; iodide

Guidance literature:: Multi-step reaction with 12 steps

1: TiCl₄ / CH₂Cl₂ / 1 h / 25 °C

2: 89 percent / KOH, NaBH₃CN / methanol / 2.5 h / 25 °C

3: 96 percent / CH₂Cl₂ / 3 h / 25 °C

4: 94 percent / Na, Fe(NO₃)*9H₂O / liquid ammonia / 4 h

5: 58 percent / NBS / benzene / 20 h / 25 °C

6: 86 percent / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 2 h; 2.) 25 deg C, 2 h

7: 78 percent / K₂CO₃, NaI / acetone / 5 h / Heating

8: 77 percent / NH₄OAc / acetic acid / 1.5 h / Heating

9: 48 percent / Cu(NO₃)2*3H₂O / acetic anhydride / 1 h / 65 °C

10: 92 percent / Fe, AcOH, silica gel / toluene / 1 h / Heating

11: H₂O; ethanol; acetic acid / 8 h / 25 °C

12: ethanol; ethyl acetate / 12 h

With potassium hydroxide; N-Bromosuccinimide; Fe(NO₃)*9H₂O; ammonium acetate; sodium; silica gel; boron tribromide; titanium tetrachloride; iron; sodium cyanoborohydride; potassium carbonate; copper(II) nitrate; acetic acid; sodium iodide; In methanol; ethanol; dichloromethane; ammonia; water; acetic anhydride; acetic acid; ethyl acetate; acetone; toluene; benzene;
DOI:10.1021/ja00311a065

Reference yield:

: 3,5-Dihydroxy-2,4-dimethyl-benzaldehyde

: 99053-80-2
(5,7-Bis-benzyloxy-4,6-dimethyl-1H-indol-3-ylmethyl)-trimethyl-ammonium; iodide

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / K₂CO₃, NaI / acetone / 5 h / Heating

2: 77 percent / NH₄OAc / acetic acid / 1.5 h / Heating

3: 48 percent / Cu(NO₃)2*3H₂O / acetic anhydride / 1 h / 65 °C

4: 92 percent / Fe, AcOH, silica gel / toluene / 1 h / Heating

5: H₂O; ethanol; acetic acid / 8 h / 25 °C

6: ethanol; ethyl acetate / 12 h

With ammonium acetate; silica gel; iron; potassium carbonate; copper(II) nitrate; acetic acid; sodium iodide; In ethanol; water; acetic anhydride; acetic acid; ethyl acetate; acetone; toluene;
DOI:10.1021/ja00311a065