4-(2-azido-1-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)phenyl acetate

Base Information

Chemical Name:4-(2-azido-1-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)phenyl acetate
CAS No.:1449417-83-7
Molecular Formula:C₁₉H₂₈N₄O₃
Molecular Weight:360.456
Hs Code.:

Synonyms:4-(2-azido-1-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)phenyl acetate

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Chemical Property of 4-(2-azido-1-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)phenyl acetate

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Technology Process of 4-(2-azido-1-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)phenyl acetate

There total 3 articles about 4-(2-azido-1-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 2628-16-2
p-acetoxystyrene

: 211562-21-9
sodium 2,2,6,6-tetramethylpiperidine-1-oxide

: 1449417-83-7
4-(2-azido-1-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)phenyl acetate

Guidance literature:: With 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In tetrahydrofuran; dichloromethane; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol402106x

Reference yield: 52.0%

: 2628-16-2
p-acetoxystyrene

: 2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate

: 1449417-83-7
4-(2-azido-1-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)phenyl acetate

Guidance literature:: With sodium azide; In acetonitrile; at 20 ℃; for 24h; under 760.051 Torr; Inert atmosphere;
DOI:10.1002/adsc.202100783

Reference yield:

: 2564-83-2
2,2,6,6-tetramethyl-piperidine-N-oxyl

: 1449417-83-7
4-(2-azido-1-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium; naphthalene / tetrahydrofuran / 20 °C / Inert atmosphere

2: 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one / tetrahydrofuran; dichloromethane / 6 h / 20 °C / Inert atmosphere

With naphthalene; sodium; 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol402106x