5-azido-3-O-benzyl-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-talofuranose

Base Information

Chemical Name:5-azido-3-O-benzyl-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-talofuranose
CAS No.:1227636-80-7
Molecular Formula:C₂₂H₃₅N₃O₅Si
Molecular Weight:449.623
Hs Code.:

Synonyms:5-azido-3-O-benzyl-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-talofuranose

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Chemical Property of 5-azido-3-O-benzyl-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-talofuranose

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Technology Process of 5-azido-3-O-benzyl-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-talofuranose

There total 8 articles about 5-azido-3-O-benzyl-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-talofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1227636-79-4
5-azido-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-talofuranose

: 100-39-0
benzyl bromide

: 1227636-80-7
5-azido-3-O-benzyl-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-talofuranose

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2010.02.063

Reference yield:

: 763122-30-1
5-azido-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-idofuranose

: 1227636-80-7
5-azido-3-O-benzyl-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-talofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium tetrahydroborate; pyridinium chlorochromate / dichloromethane; ethanol / Molecular sieve

2: N,N-dimethyl-formamide

With sodium tetrahydroborate; water; pyridinium chlorochromate; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 130619-55-5
5-azido-5-deoxy-1,2-O-isopropylidene-β-L-idofuranose

: 1227636-80-7
5-azido-3-O-benzyl-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-talofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: water; sodium tetrahydroborate; pyridinium chlorochromate / dichloromethane; ethanol / Molecular sieve

3: N,N-dimethyl-formamide

With pyridine; sodium tetrahydroborate; water; pyridinium chlorochromate; In ethanol; dichloromethane; N,N-dimethyl-formamide;