8,9-dihydro-3,11-diisopropoxy-14-(3-isopropoxy-4-methoxyphenyl)-2,12-dimethoxy-6H-[1]benzopyrano[4′,3′:4,5]pyrrolo[2,1-α]isoquinolin-6-one

Base Information

Chemical Name:8,9-dihydro-3,11-diisopropoxy-14-(3-isopropoxy-4-methoxyphenyl)-2,12-dimethoxy-6H-[1]benzopyrano[4′,3′:4,5]pyrrolo[2,1-α]isoquinolin-6-one
CAS No.:271243-11-9
Molecular Formula:C₃₇H₄₁NO₈
Molecular Weight:627.734
Hs Code.:

Synonyms:8,9-dihydro-3,11-diisopropoxy-14-(3-isopropoxy-4-methoxyphenyl)-2,12-dimethoxy-6H-[1]benzopyrano[4′,3′:4,5]pyrrolo[2,1-α]isoquinolin-6-one

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Chemical Property of 8,9-dihydro-3,11-diisopropoxy-14-(3-isopropoxy-4-methoxyphenyl)-2,12-dimethoxy-6H-[1]benzopyrano[4′,3′:4,5]pyrrolo[2,1-α]isoquinolin-6-one

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Technology Process of 8,9-dihydro-3,11-diisopropoxy-14-(3-isopropoxy-4-methoxyphenyl)-2,12-dimethoxy-6H-[1]benzopyrano[4′,3′:4,5]pyrrolo[2,1-α]isoquinolin-6-one

There total 50 articles about 8,9-dihydro-3,11-diisopropoxy-14-(3-isopropoxy-4-methoxyphenyl)-2,12-dimethoxy-6H-[1]benzopyrano[4′,3′:4,5]pyrrolo[2,1-α]isoquinolin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 3-[2-(2-Bromo-5-isopropoxy-4-methoxyphenyl)ethyl]-7-isopropoxy-1-(3-isopropoxy-4-methoxyphenyl)-8-methoxy-4-oxo-3H-[1]benzopyrano[3,4-b]pyrrole-2-carboxylic acid

: 271243-11-9
8,9-dihydro-3,11-diisopropoxy-14-(3-isopropoxy-4-methoxyphenyl)-2,12-dimethoxy-6H-[1]benzopyrano[4′,3′:4,5]pyrrolo[2,1-α]isoquinolin-6-one

Guidance literature:: With triethylamine; triphenylphosphine; palladium diacetate; In acetonitrile; at 150 ℃; for 1.33333h;
DOI:10.1002/(SICI)1521-3765(20000403)6:7<1147::AID-CHEM1147<3.3.CO;2-T

Reference yield: 90.0%

: 875654-31-2
7-isopropoxy-1-(3-isopropoxy-4-methoxyphenyl)-3-[2-(3-isopropoxy-4-methoxyphenyl)ethyl]-8-methoxy-4-oxo-[1]benzopyrano[3,4-b]pyrrol-4(3H)-one

: 271243-11-9
8,9-dihydro-3,11-diisopropoxy-14-(3-isopropoxy-4-methoxyphenyl)-2,12-dimethoxy-6H-[1]benzopyrano[4′,3′:4,5]pyrrolo[2,1-α]isoquinolin-6-one

Guidance literature:: With boron trifluoride diethyl etherate; bis-[(trifluoroacetoxy)iodo]benzene; In dichloromethane; at -40 ℃; for 1.5h;
DOI:10.1016/j.tet.2005.10.014

Reference yield: 80.0%

: 660397-48-8
14-bromo-3,11-diisopropoxy-2,12-dimethoxy-8,9-dihydro-6H-[1]benzopyrano[4’,3’:4,5]pyrrolo[2,1-a]isoquinolin-6-one

: 516465-82-0
(3-isopropoxy-4-methoxyphenyl)boronic acid

: 271243-11-9
8,9-dihydro-3,11-diisopropoxy-14-(3-isopropoxy-4-methoxyphenyl)-2,12-dimethoxy-6H-[1]benzopyrano[4′,3′:4,5]pyrrolo[2,1-α]isoquinolin-6-one

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride; silver(l) oxide; In 1,2-dimethoxyethane; at 85 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jm400719y