4-amino-5-cyano-6-oxo-3-formamido-N-(4-oxo-2-thioxothiazolidin-3-yl)-1-phenylpyridazine

Base Information

Chemical Name:4-amino-5-cyano-6-oxo-3-formamido-N-(4-oxo-2-thioxothiazolidin-3-yl)-1-phenylpyridazine
CAS No.:439943-72-3
Molecular Formula:C₁₅H₁₀N₆O₃S₂
Molecular Weight:386.415
Hs Code.:

Synonyms:4-amino-5-cyano-6-oxo-3-formamido-N-(4-oxo-2-thioxothiazolidin-3-yl)-1-phenylpyridazine

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Chemical Property of 4-amino-5-cyano-6-oxo-3-formamido-N-(4-oxo-2-thioxothiazolidin-3-yl)-1-phenylpyridazine

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Technology Process of 4-amino-5-cyano-6-oxo-3-formamido-N-(4-oxo-2-thioxothiazolidin-3-yl)-1-phenylpyridazine

There total 2 articles about 4-amino-5-cyano-6-oxo-3-formamido-N-(4-oxo-2-thioxothiazolidin-3-yl)-1-phenylpyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-39-5
chloroacetic acid ethyl ester

: C₁₃H₉N₆O₂S₂^(1-)*K⁽¹⁺⁾

: 439943-72-3
4-amino-5-cyano-6-oxo-3-formamido-N-(4-oxo-2-thioxothiazolidin-3-yl)-1-phenylpyridazine

Guidance literature:: chloroacetic acid ethyl ester; C₁₃H₉N₆O₂S₂^(1-)*K⁽¹⁺⁾; In N,N-dimethyl-formamide; at 0 ℃;

With hydrogenchloride; In N,N-dimethyl-formamide; pH=6;

Reference yield:

: 82754-66-3
4-amino-5-cyano-3-hydrazinocarbonyl-6-oxo-1-phenyl-1,6-dihydropyridazine

: 439943-72-3
4-amino-5-cyano-6-oxo-3-formamido-N-(4-oxo-2-thioxothiazolidin-3-yl)-1-phenylpyridazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: KOH / dimethylformamide / 1 h / 70 °C

2.1: dimethylformamide / 0 °C

2.2: 2.9 g / HCl / dimethylformamide / pH 6

With potassium hydroxide; In N,N-dimethyl-formamide;