N₆-cyclohexyl-N₂-[2-methoxy-4-(1,2,3,6-tetrahydropyridin-4-yl)phenyl]-9H-purine-2,6-diamine

Base Information

• Chemical Name: N₆-cyclohexyl-N₂-[2-methoxy-4-(1,2,3,6-tetrahydropyridin-4-yl)phenyl]-9H-purine-2,6-diamine
• CAS No.: 1246533-08-3
• Molecular Formula: C₂₃H₂₉N₇O
• Molecular Weight: 419.53

Synonyms:N₆-cyclohexyl-N₂-[2-methoxy-4-(1,2,3,6-tetrahydropyridin-4-yl)phenyl]-9H-purine-2,6-diamine

Chemical Property of N₆-cyclohexyl-N₂-[2-methoxy-4-(1,2,3,6-tetrahydropyridin-4-yl)phenyl]-9H-purine-2,6-diamine

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Technology Process of N₆-cyclohexyl-N₂-[2-methoxy-4-(1,2,3,6-tetrahydropyridin-4-yl)phenyl]-9H-purine-2,6-diamine

There total 1 articles about N₆-cyclohexyl-N₂-[2-methoxy-4-(1,2,3,6-tetrahydropyridin-4-yl)phenyl]-9H-purine-2,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 4-[4-[[6-(cyclohexylamino)-9-tetrahydropyran-2-yl-purin-2-yl]amino]-3-methoxy-phenyl]-3,6-dihydro-2H-pyridine-1-carboxylate (1246533-07-2) → N6-cyclohexyl-N2-[2-methoxy-4-(1,2,3,6-tetrahydropyridin-4-yl)phenyl]-9H-purine-2,6-diamine (1246533-08-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 4h;

Reference yield:

N6-cyclohexyl-N2-[2-methoxy-4-(1,2,3,6-tetrahydropyridin-4-yl)phenyl]-9H-purine-2,6-diamine (1246533-08-3) + methanesulfonyl chloride (124-63-0) → N6-cyclohexyl-N2-{2-methoxy-4-[1-(methylsulfonyl)-1,2,3,6-tetrahydropyridin-4-yl]phenyl}-9H-purine-2,6-diamine (1246531-74-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

1-Methyl-cyclopropanoic acid (6914-76-7) + N6-cyclohexyl-N2-[2-methoxy-4-(1,2,3,6-tetrahydropyridin-4-yl)phenyl]-9H-purine-2,6-diamine (1246533-08-3) → [4-(4-{[6-(cyclohexylamino)-9H-purin-2-yl]amino}-3-methoxyphenyl)-3,6-dihydropyridin-1(2H)-yl](1-methylcyclopropyl)methanone (1246531-72-5)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

upstream raw materials:

tert-butyl 4-[4-[[6-(cyclohexylamino)-9-tetrahydropyran-2-yl-purin-2-yl]amino]-3-methoxy-phenyl]-3,6-dihydro-2H-pyridine-1-carboxylate

Downstream raw materials:

N₆-cyclohexyl-N₂-{2-methoxy-4-[1-(methylsulfonyl)-1,2,3,6-tetrahydropyridin-4-yl]phenyl}-9H-purine-2,6-diamine

[4-(4-{[6-(cyclohexylamino)-9H-purin-2-yl]amino}-3-methoxyphenyl)-3,6-dihydropyridin-1(2H)-yl](1-methylcyclopropyl)methanone

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