2-[2-(2-bromobenzyloxy)phenyl]-[1,3]dithiane

Base Information

• Chemical Name: 2-[2-(2-bromobenzyloxy)phenyl]-[1,3]dithiane
• CAS No.: 1030614-23-3
• Molecular Formula: C₁₇H₁₇BrOS₂
• Molecular Weight: 381.357
• Mol file: 1030614-23-3.mol

Synonyms:2-[2-(2-bromobenzyloxy)phenyl]-[1,3]dithiane

Chemical Property of 2-[2-(2-bromobenzyloxy)phenyl]-[1,3]dithiane

Chemical Property:

Purity/Quality:

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Technology Process of 2-[2-(2-bromobenzyloxy)phenyl]-[1,3]dithiane

There total 1 articles about 2-[2-(2-bromobenzyloxy)phenyl]-[1,3]dithiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-(2-hydroxyphenyl)-1,3-dithiane (6842-36-0) + 2-Iodobenzyl bromide (40400-13-3) → 2-[2-(2-bromobenzyloxy)phenyl]-[1,3]dithiane (1030614-23-3)

Guidance literature:

With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1002/ejoc.200700762

Reference yield: 80.0%

2-[2-(2-bromobenzyloxy)phenyl]-[1,3]dithiane (1030614-23-3) → [2-(2-bromobenzyloxy)phenyl]methanol (1020929-37-6)

Guidance literature:

2-[2-(2-bromobenzyloxy)phenyl]-[1,3]dithiane; With methyl iodide; In water; acetonitrile; at 25 ℃; for 12h;

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 2h; Further stages.;

DOI:10.1002/ejoc.200700762

upstream raw materials:

2-(2-hydroxyphenyl)-1,3-dithiane

2-Iodobenzyl bromide

Downstream raw materials:

[2-(2-bromobenzyloxy)phenyl]methanol