C₅H₁₁OC₆H₃CHOOH

Base Information

• Chemical Name: C₅H₁₁OC₆H₃CHOOH
• CAS No.: 291507-15-8
• Molecular Formula: C₁₂H₁₆O₃
• Molecular Weight: 208.257
• Mol file: 291507-15-8.mol

Synonyms:C₅H₁₁OC₆H₃CHOOH

Chemical Property of C₅H₁₁OC₆H₃CHOOH

Chemical Property:

Purity/Quality:

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Technology Process of C₅H₁₁OC₆H₃CHOOH

There total 1 articles about C₅H₁₁OC₆H₃CHOOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

2,5-Dihydroxybenzaldehyde (1194-98-5) + 1-Bromopentane (110-53-2) → C5H11OC6H3CHOOH (291507-15-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1016/j.cclet.2020.03.079

Reference yield:

C5H11OC6H3CHOOH (291507-15-8) + propargyl bromide (106-96-7) → C15H18O3

Guidance literature:

With potassium carbonate; In acetonitrile; for 15h; Reflux; Sealed tube;

DOI:10.1016/j.cclet.2020.03.079

Reference yield:

C5H11OC6H3CHOOH (291507-15-8) → C15H20O3

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 15 h / Reflux; Sealed tube

2: sodium tetrahydroborate; methanol / 0.08 h / 20 °C

With methanol; sodium tetrahydroborate; potassium carbonate; In acetonitrile;

DOI:10.1016/j.cclet.2020.03.079

upstream raw materials:

2,5-Dihydroxybenzaldehyde

1-Bromopentane