xyloidone

Base Information

Chemical Name:xyloidone
CAS No.:15297-92-4
Molecular Formula:C15H12O3
Molecular Weight:240.258
Hs Code.:2914399090
Mol file:15297-92-4.mol

Synonyms:Dehydro-a-lapachol;Dehydro-a-lapachone;Dehydro-a-lapacone;Dehydrolapachone;NSC106453;NSC 629748;Xiloidone;Xyloidone;a-Lapachone, dehydro-;

Suppliers and Price of xyloidone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
Q 99 2,2-DIMETHYL-2H-NAPHTHO(2,3-B)PYRAN-5,10-DIONE Aldrich
100mg
$ 144.00

Crysdot
Dehydro-α-lapachone 95+%
100mg
$ 125.00

Arctom
Dehydro-alpha-lapachone
5mg
$ 373.00

Arctom
Dehydro-alpha-Lapachone ≥98%
5mg
$ 226.00

Total 37 raw suppliers

Chemical Property of xyloidone

Chemical Property:

Vapor Pressure:1.87E-06mmHg at 25°C
Melting Point:156 °C
Refractive Index:1.62
Boiling Point:395.2 °C at 760 mmHg
Flash Point:177 °C
PSA：43.37000
Density:1.28 g/cm³
LogP:2.68470
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

Q 99 2,2-DIMETHYL-2H-NAPHTHO(2,3-B)PYRAN-5,10-DIONE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of xyloidone

There total 36 articles about xyloidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.1%

: 861216-48-0
tert-butyl 2-methylbut-3-en-2-yl carbonate

: 83-72-7
2-hydroxynaphtho-1,4-quinone

: 15297-92-4
2,2-dimethyl-2H-benzo[g]chromene-5,10-dione

Guidance literature:: With cerium(III) chloride; bis(acetylacetonato)palladium(II); potassium acetate; copper(II) bis(trifluoromethanesulfonate); acetic acid; 1-hexyl-3-methylimidazol-1-ium chloride; at 20 ℃; for 2.5h; Reagent/catalyst;

Reference yield: 91.0%

: 83-72-7
2-hydroxynaphtho-1,4-quinone

: 107-86-8
3,3-dimethyl acrylaldehyde

: 15297-92-4
2,2-dimethyl-2H-benzo[g]chromene-5,10-dione

Guidance literature:: In neat (no solvent); at 20 - 120 ℃; for 12h; Microwave irradiation; Green chemistry;
DOI:10.5012/bkcs.2013.34.10.2963

Reference yield: 89.0%

: 1111-97-3
3-chloro-3-methylbut-1-yne

: 83-72-7
2-hydroxynaphtho-1,4-quinone

: 15297-92-4
2,2-dimethyl-2H-benzo[g]chromene-5,10-dione

Guidance literature:: With iodine; 1,8-diazabicyclo[5.4.0]undec-7-ene; copper dichloride; In acetonitrile; for 24h; Concentration; Reflux;
DOI:10.1002/jhet.2087