ethyl 2,3,6-tri-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 2,3,6-tri-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-1-thio-β-D-glucopyranoside
CAS No.:1397680-26-0
Molecular Formula:C₄₄H₄₄O₇S
Molecular Weight:716.895
Hs Code.:

Synonyms:ethyl 2,3,6-tri-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-1-thio-β-D-glucopyranoside

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Chemical Property of ethyl 2,3,6-tri-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-1-thio-β-D-glucopyranoside

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Technology Process of ethyl 2,3,6-tri-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-1-thio-β-D-glucopyranoside

There total 1 articles about ethyl 2,3,6-tri-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 141263-02-7
ethyl 2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 1397680-26-0
ethyl 2,3,6-tri-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-1-thio-β-D-glucopyranoside

Guidance literature:: ethyl 2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside; With pyridine; In dichloromethane; for 0.5h; Cooling with ice;

(fluorenylmethoxy)carbonyl chloride; In dichloromethane; at 20 ℃; for 6h; Cooling with ice;
DOI:10.1021/jacs.1c02188

Reference yield: 70.0%

: 1397680-26-0
ethyl 2,3,6-tri-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-1-thio-β-D-glucopyranoside

: C₄₂H₄₀O₈

Guidance literature:: With hydrogenchloride; N-Bromosuccinimide; In tetrahydrofuran; water;
DOI:10.1016/j.chembiol.2011.03.009

Reference yield:

: 1397680-26-0
ethyl 2,3,6-tri-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-1-thio-β-D-glucopyranoside

: benzyl 2-O-benzoyl-3,6-O-dibenzyl-β-D-glucopyranoside

: C₇₆H₇₂O₁₄

: C₇₆H₇₂O₁₄

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -15 - 0 ℃; for 1.08333h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1021/jacs.1c02188