(+/-)-(1α,2β,3β,4α)-4-<<2-amino-6-chloro-5-<(4-chlorophenyl)azo>pyrimidin-2-yl>amino>-2,3-O-isopropylidene-1,2,3-cyclopentanetriol

Base Information

Chemical Name:(+/-)-(1α,2β,3β,4α)-4-<<2-amino-6-chloro-5-<(4-chlorophenyl)azo>pyrimidin-2-yl>amino>-2,3-O-isopropylidene-1,2,3-cyclopentanetriol
CAS No.:135700-57-1
Molecular Formula:C₁₈H₂₀Cl₂N₆O₃
Molecular Weight:439.301
Hs Code.:

Synonyms:(+/-)-(1α,2β,3β,4α)-4-<<2-amino-6-chloro-5-<(4-chlorophenyl)azo>pyrimidin-2-yl>amino>-2,3-O-isopropylidene-1,2,3-cyclopentanetriol

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Chemical Property of (+/-)-(1α,2β,3β,4α)-4-<<2-amino-6-chloro-5-<(4-chlorophenyl)azo>pyrimidin-2-yl>amino>-2,3-O-isopropylidene-1,2,3-cyclopentanetriol

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Technology Process of (+/-)-(1α,2β,3β,4α)-4-<<2-amino-6-chloro-5-<(4-chlorophenyl)azo>pyrimidin-2-yl>amino>-2,3-O-isopropylidene-1,2,3-cyclopentanetriol

There total 2 articles about (+/-)-(1α,2β,3β,4α)-4-<<2-amino-6-chloro-5-<(4-chlorophenyl)azo>pyrimidin-2-yl>amino>-2,3-O-isopropylidene-1,2,3-cyclopentanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2028-74-2
p-chlorobenzenediazonium chloride

: 135700-56-0
(+/-)-(1α,2β,3β,4α)-4-<(2-Amino-6-chloropyrimidin-4-yl)amino>-2,3-O-isopropylidene-1,2,3-cyclopentanetriol

: 135700-57-1
(+/-)-(1α,2β,3β,4α)-4-<<2-amino-6-chloro-5-<(4-chlorophenyl)azo>pyrimidin-2-yl>amino>-2,3-O-isopropylidene-1,2,3-cyclopentanetriol

Guidance literature:: With hydrogenchloride; sodium acetate; acetic acid; In water; for 40h; Ambient temperature;
DOI:10.1021/jm00096a012

Reference yield:

: 88756-83-6
(+/-)-1β-amino-2α,3α-O-isopropylidene-2α,3α,4β-cyclopentanetriol

: 135700-57-1
(+/-)-(1α,2β,3β,4α)-4-<<2-amino-6-chloro-5-<(4-chlorophenyl)azo>pyrimidin-2-yl>amino>-2,3-O-isopropylidene-1,2,3-cyclopentanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Et₃N / butan-1-ol / 48 h / Heating

2: 92 percent / sodium acetate trihydrate, glacial acetic acid, 12 N aq. HCl / H₂O / 40 h / Ambient temperature

With hydrogenchloride; sodium acetate; acetic acid; triethylamine; In water; butan-1-ol;
DOI:10.1021/jm00096a012