trans-[PtCl₂(N=C(Me)O-N(Me)-C(H)Ph)2]

Base Information

Chemical Name:trans-[PtCl₂(N=C(Me)O-N(Me)-C(H)Ph)2]
CAS No.:324764-91-2
Molecular Formula:C₂₀H₂₄Cl₂N₄O₂Pt
Molecular Weight:618.422
Hs Code.:

trans-[PtCl<sub>2</sub>(N=C(Me)O-N(Me)-C(H)Ph)2]

Synonyms:trans-[PtCl₂(N=C(Me)O-N(Me)-C(H)Ph)2]

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Chemical Property of trans-[PtCl₂(N=C(Me)O-N(Me)-C(H)Ph)2]

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Technology Process of trans-[PtCl₂(N=C(Me)O-N(Me)-C(H)Ph)2]

There total 2 articles about trans-[PtCl₂(N=C(Me)O-N(Me)-C(H)Ph)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 270064-62-5,267238-07-3
(PtCl₄(NC(CH₃)ON(CH₃)CHC₆H₅)2)

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 324764-91-2
(PtCl₂(NC(CH₃)ON(CH₃)CHC₆H₅)2)

: 2181-97-7
(2-methoxy-2-oxoethyl)triphenylphosphonium chloride

: 791-28-6
Triphenylphosphine oxide

Guidance literature:: In dichloromethane; Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent;
DOI:10.1021/ic000769c

Reference yield: 56.0%

: 267238-07-3,270064-62-5
trans-[PtCl₄(N=C(Me)O-N(Me)-C(H)(Ph))2]

: 324764-91-2
trans-[PtCl₂(N=C(Me)O-N(Me)-C(H)Ph)2]

Guidance literature:: With C₆H₅CH₂NHOH*HCl; NaHCO₃; H₂O; In dichloromethane; a drop of H2O added to slurry of Pt complex, PhCH2NHOH*HCl, and NaHCO3 in CH2Cl2, stirred at 20-25°C for 12 h; solvent removed (vac.), residue chromd. (SiO2, CH2Cl2); elem. anal.;
DOI:10.1021/ic000477b

Reference yield: 99.0%

: 324764-91-2
trans-[PtCl₂(N=C(Me)O-N(Me)-C(H)Ph)2]

: 7782-50-5
chlorine

: 267238-07-3,270064-62-5
trans-[PtCl₄(N=C(Me)O-N(Me)-C(H)(Ph))2]

Guidance literature:: In chloroform-d1; an excess of Cl2 passed through complex soln. at room temp. for 10-15 s; not isolated, detected by NMR after 5 min;
DOI:10.1021/ic000477b