(1R,3S,4S,5S,7R,9R,10R,11R)-1,9-diacetyloxy-7-p-nitrobenzoyloxylongipinane

Base Information

Chemical Name:(1R,3S,4S,5S,7R,9R,10R,11R)-1,9-diacetyloxy-7-p-nitrobenzoyloxylongipinane
CAS No.:471861-81-1
Molecular Formula:C₂₆H₃₃NO₈
Molecular Weight:487.55
Hs Code.:

Synonyms:(1R,3S,4S,5S,7R,9R,10R,11R)-1,9-diacetyloxy-7-p-nitrobenzoyloxylongipinane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,3S,4S,5S,7R,9R,10R,11R)-1,9-diacetyloxy-7-p-nitrobenzoyloxylongipinane

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Technology Process of (1R,3S,4S,5S,7R,9R,10R,11R)-1,9-diacetyloxy-7-p-nitrobenzoyloxylongipinane

There total 3 articles about (1R,3S,4S,5S,7R,9R,10R,11R)-1,9-diacetyloxy-7-p-nitrobenzoyloxylongipinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75-36-5
acetyl chloride

: 471861-78-6
(1R,3S,4S,5S,7R,9R,10R,11R)-1,9-dihydroxy-7-p-nitrobenzoyloxylongipinane

: 471861-81-1
(1R,3S,4S,5S,7R,9R,10R,11R)-1,9-diacetyloxy-7-p-nitrobenzoyloxylongipinane

Guidance literature:: for 0.166667h; Heating;
DOI:10.1021/np020158s

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 471861-81-1
(1R,3S,4S,5S,7R,9R,10R,11R)-1,9-diacetyloxy-7-p-nitrobenzoyloxylongipinane

Guidance literature:: Multi-step reaction with 2 steps

1: 10 percent / pyridine / 24 h / 4 °C

2: 95 percent / 0.17 h / Heating

With pyridine;
DOI:10.1021/np020158s

Reference yield:

: 97335-22-3
3-epi-longipinane-1β,7β,9α-triol

: 471861-81-1
(1R,3S,4S,5S,7R,9R,10R,11R)-1,9-diacetyloxy-7-p-nitrobenzoyloxylongipinane

Guidance literature:: Multi-step reaction with 2 steps

1: 10 percent / pyridine / 24 h / 4 °C

2: 95 percent / 0.17 h / Heating

With pyridine;
DOI:10.1021/np020158s