methyl 2-methoxy-4-((1S,4R)-3-oxo-2-azabicyclo[2.2.1]heptan-2-yl)benzoate

Base Information

Chemical Name:methyl 2-methoxy-4-((1S,4R)-3-oxo-2-azabicyclo[2.2.1]heptan-2-yl)benzoate
CAS No.:1311258-55-5
Molecular Formula:C₁₅H₁₇NO₄
Molecular Weight:275.304
Hs Code.:

Synonyms:methyl 2-methoxy-4-((1S,4R)-3-oxo-2-azabicyclo[2.2.1]heptan-2-yl)benzoate

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Chemical Property of methyl 2-methoxy-4-((1S,4R)-3-oxo-2-azabicyclo[2.2.1]heptan-2-yl)benzoate

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Technology Process of methyl 2-methoxy-4-((1S,4R)-3-oxo-2-azabicyclo[2.2.1]heptan-2-yl)benzoate

There total 3 articles about methyl 2-methoxy-4-((1S,4R)-3-oxo-2-azabicyclo[2.2.1]heptan-2-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1311258-54-4
methyl 2-methoxy-4-((1R,4S)-3-oxo-2-azabicyclo[2.2.1]hept-5-en-2-yl)benzoate

: 1311258-55-5
methyl 2-methoxy-4-((1S,4R)-3-oxo-2-azabicyclo[2.2.1]heptan-2-yl)benzoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 6h;

Reference yield:

: 148490-97-5
4-iodo-2-methoxybenzoic acid-methyl ester

: 1311258-55-5
methyl 2-methoxy-4-((1S,4R)-3-oxo-2-azabicyclo[2.2.1]heptan-2-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate / copper(l) iodide; N,N`-dimethylethylenediamine / toluene / 18 h / 110 °C / Inert atmosphere

2: hydrogen / palladium on activated charcoal / ethyl acetate / 6 h / 20 °C

With potassium phosphate; hydrogen; copper(l) iodide; palladium on activated charcoal; N,N`-dimethylethylenediamine; In ethyl acetate; toluene;

Reference yield:

: 89942-34-7
2-methoxy-4-iodobenzoic acid

: 1311258-55-5
methyl 2-methoxy-4-((1S,4R)-3-oxo-2-azabicyclo[2.2.1]heptan-2-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 18 h / 0 - 20 °C / Inert atmosphere

2: potassium phosphate / copper(l) iodide; N,N`-dimethylethylenediamine / toluene / 18 h / 110 °C / Inert atmosphere

3: hydrogen / palladium on activated charcoal / ethyl acetate / 6 h / 20 °C

With potassium phosphate; thionyl chloride; hydrogen; copper(l) iodide; palladium on activated charcoal; N,N`-dimethylethylenediamine; In ethyl acetate; toluene;