methyl 2-methoxy-4-((1R,4S)-3-oxo-2-azabicyclo[2.2.1]hept-5-en-2-yl)benzoate

Base Information

Chemical Name:methyl 2-methoxy-4-((1R,4S)-3-oxo-2-azabicyclo[2.2.1]hept-5-en-2-yl)benzoate
CAS No.:1311258-54-4
Molecular Formula:C₁₅H₁₅NO₄
Molecular Weight:273.288
Hs Code.:

Synonyms:methyl 2-methoxy-4-((1R,4S)-3-oxo-2-azabicyclo[2.2.1]hept-5-en-2-yl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-methoxy-4-((1R,4S)-3-oxo-2-azabicyclo[2.2.1]hept-5-en-2-yl)benzoate

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Technology Process of methyl 2-methoxy-4-((1R,4S)-3-oxo-2-azabicyclo[2.2.1]hept-5-en-2-yl)benzoate

There total 2 articles about methyl 2-methoxy-4-((1R,4S)-3-oxo-2-azabicyclo[2.2.1]hept-5-en-2-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 79200-56-9
(-)-2-azabicyclo[2.2.1]hept-5-en-3-one

: 148490-97-5
4-iodo-2-methoxybenzoic acid-methyl ester

: 1311258-54-4
methyl 2-methoxy-4-((1R,4S)-3-oxo-2-azabicyclo[2.2.1]hept-5-en-2-yl)benzoate

Guidance literature:: With potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine; In toluene; at 110 ℃; for 18h; Inert atmosphere;

Reference yield:

: 89942-34-7
2-methoxy-4-iodobenzoic acid

: 1311258-54-4
methyl 2-methoxy-4-((1R,4S)-3-oxo-2-azabicyclo[2.2.1]hept-5-en-2-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 18 h / 0 - 20 °C / Inert atmosphere

2: potassium phosphate / copper(l) iodide; N,N`-dimethylethylenediamine / toluene / 18 h / 110 °C / Inert atmosphere

With potassium phosphate; thionyl chloride; copper(l) iodide; N,N`-dimethylethylenediamine; In toluene;