4,6-bis(4-chlorophenyl)-2-((2,3,4,5,6-pentahydroxyhexylidene)hydrazinyl)nicotinonitrile

Base Information

• Chemical Name: 4,6-bis(4-chlorophenyl)-2-((2,3,4,5,6-pentahydroxyhexylidene)hydrazinyl)nicotinonitrile
• CAS No.: 1416954-85-2
• Molecular Formula: C₂₄H₂₂Cl₂N₄O₅
• Molecular Weight: 517.368

Synonyms:4,6-bis(4-chlorophenyl)-2-((2,3,4,5,6-pentahydroxyhexylidene)hydrazinyl)nicotinonitrile

Chemical Property of 4,6-bis(4-chlorophenyl)-2-((2,3,4,5,6-pentahydroxyhexylidene)hydrazinyl)nicotinonitrile

Chemical Property:

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Technology Process of 4,6-bis(4-chlorophenyl)-2-((2,3,4,5,6-pentahydroxyhexylidene)hydrazinyl)nicotinonitrile

There total 6 articles about 4,6-bis(4-chlorophenyl)-2-((2,3,4,5,6-pentahydroxyhexylidene)hydrazinyl)nicotinonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

D-glucose (50-99-7) + 4,6-bis(4-chlorophenyl)-2-hydrazinylnicotinonitrile (1416954-77-2) → 4,6-bis(4-chlorophenyl)-2-((2,3,4,5,6-pentahydroxyhexylidene)hydrazinyl)nicotinonitrile (1416954-85-2)

Guidance literature:

With acetic acid; In ethanol; at 80 ℃; for 2h;

DOI:10.1002/jhet.966

Reference yield:

4-chlorobenzaldehyde (104-88-1) → 4,6-bis(4-chlorophenyl)-2-((2,3,4,5,6-pentahydroxyhexylidene)hydrazinyl)nicotinonitrile (1416954-85-2)

Guidance literature:

Multi-step reaction with 4 steps

1: ammonium acetate; acetic acid / 3 h / Reflux

2: potassium carbonate / acetone / 20 h / Reflux

3: hydrazine hydrate / ethanol / 6 h / Reflux

4: acetic acid / ethanol / 2 h / 80 °C

With ammonium acetate; potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; acetone;

DOI:10.1002/jhet.966

Reference yield:

1,3-bis(4-chlorophenyl)prop-2-en-1-one (20725-25-1,22966-30-9,19672-59-4) → 4,6-bis(4-chlorophenyl)-2-((2,3,4,5,6-pentahydroxyhexylidene)hydrazinyl)nicotinonitrile (1416954-85-2)

Guidance literature:

Multi-step reaction with 4 steps

1: ammonium acetate / ethanol / 10 h / Reflux

2: potassium carbonate / acetone / 20 h / Reflux

3: hydrazine hydrate / ethanol / 6 h / Reflux

4: acetic acid / ethanol / 2 h / 80 °C

With ammonium acetate; potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; acetone;

DOI:10.1002/jhet.966

upstream raw materials:

para-chloroacetophenone

1,3-bis(4-chlorophenyl)prop-2-en-1-one

4-chlorobenzaldehyde

4,6-bis-(4-chloro-phenyl)-2-oxo-1,2-dihydro-pyridine-3-carbonitrile

Downstream raw materials:

6-(2-[4,6-bis(4-chlorophenyl)-3-cyanopyridin-2-yl]hydrazono)hexane-1,2,3,4,5-pentayl pentaacetate

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