2-[3-(3,4-dimethoxy-phenyl)-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate

Base Information

Chemical Name:2-[3-(3,4-dimethoxy-phenyl)-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate
CAS No.:167262-73-9
Molecular Formula:C₂₅H₃₃NO₉S
Molecular Weight:523.604
Hs Code.:

Synonyms:2-[3-(3,4-dimethoxy-phenyl)-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate

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Chemical Property of 2-[3-(3,4-dimethoxy-phenyl)-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate

Chemical Property:

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Technology Process of 2-[3-(3,4-dimethoxy-phenyl)-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate

There total 4 articles about 2-[3-(3,4-dimethoxy-phenyl)-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 167262-72-8
1-(3,4,5-trimethoxy-benzoyl)-3-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-ethyl)-pyrrolidine

: 124-63-0
methanesulfonyl chloride

: 167262-73-9
2-[3-(3,4-dimethoxy-phenyl)-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate

Guidance literature:: With hydrogenchloride; sodium hydrogencarbonate; triethylamine; In dichloromethane;

Reference yield:

: 167262-72-8
1-(3,4,5-trimethoxy-benzoyl)-3-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-ethyl)-pyrrolidine

: 124-63-0
methanesulfonyl chloride

: 167262-73-9
2-[3-(3,4-dimethoxy-phenyl)-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate

Guidance literature:: With hydrogenchloride; sodium hydrogencarbonate; trimethylamine; In dichloromethane;

Reference yield:

: 52424-57-4
3-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-ethyl)-pyrrolidine

: 167262-73-9
2-[3-(3,4-dimethoxy-phenyl)-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; sodium chloride; sodium hydrogencarbonate; sodium carbonate; potassium carbonate / dichloromethane; water; ethyl acetate

2: hydrogenchloride; sodium hydrogencarbonate; trimethylamine / dichloromethane

With hydrogenchloride; sodium chloride; sodium hydrogencarbonate; sodium carbonate; potassium carbonate; trimethylamine; In dichloromethane; water; ethyl acetate;