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6-(tritylthio)hexyl methanesulphonate

Base Information
  • Chemical Name:6-(tritylthio)hexyl methanesulphonate
  • CAS No.:1292765-41-3
  • Molecular Formula:C26H30O3S2
  • Molecular Weight:454.654
  • Hs Code.:
6-(tritylthio)hexyl methanesulphonate

Synonyms:6-(tritylthio)hexyl methanesulphonate

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Chemical Property of 6-(tritylthio)hexyl methanesulphonate
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Technology Process of 6-(tritylthio)hexyl methanesulphonate

There total 1 articles about 6-(tritylthio)hexyl methanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With triethylamine; In dichloromethane; at -10 ℃; Inert atmosphere;
DOI:10.1021/ja108807j
Guidance literature:
With potassium carbonate; In acetonitrile; at 80 ℃; for 25h; Inert atmosphere;
DOI:10.1021/acs.jmedchem.6b00084
Guidance literature:
Multi-step reaction with 2 steps
1: potassium carbonate / ethanol / 14 h / Inert atmosphere; Reflux
2: trifluoroacetic acid / dichloromethane / 1 h / Inert atmosphere
With potassium carbonate; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1021/ja108807j
upstream raw materials:

methanesulfonyl chloride

6-S-trityl-6-mercapto-1-hexanol

Downstream raw materials:

C15H25NS

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