as-Triazine, 5,6-dimethyl-3-methoxy-

Base Information

• Chemical Name: as-Triazine, 5,6-dimethyl-3-methoxy-
• CAS No.: 28735-31-1
• Molecular Formula: C₆H₉N₃O
• Molecular Weight: 139.157
• Hs Code.: 2933699090
• DSSTox Substance ID: DTXSID60182896
• Nikkaji Number: J90.993I
• Wikidata: Q83053594
• Mol file: 28735-31-1.mol

Synonyms:as-Triazine, 5,6-dimethyl-3-methoxy-;BRN 0742867;28735-31-1;5,6-Dimethyl-3-methoxy-as-triazine;3-methoxy-5,6-dimethyl-1,2,4-triazine;1,2,4-Triazine, 3-methoxy-5,6-dimethyl-;SCHEMBL11278139;DTXSID60182896;AKOS006278710;LS-155367

Chemical Property of as-Triazine, 5,6-dimethyl-3-methoxy-

Chemical Property:

• Vapor Pressure: 0.0274mmHg at 25°C
• Boiling Point: 254.5°C at 760 mmHg
• Flash Point: 93.1°C
• PSA: 47.90000
• Density: 1.107g/cm³
• LogP: 0.49700
• XLogP3: 0.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 139.074561919
• Heavy Atom Count: 10
• Complexity: 109

Purity/Quality:

5,6-DIMETHYL-3-METHOXY-AS-TRIAZINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(N=NC(=N1)OC)C

Technology Process of as-Triazine, 5,6-dimethyl-3-methoxy-

There total 2 articles about as-Triazine, 5,6-dimethyl-3-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium methylate (124-41-4) + 3-methylthio-5,6-dimethyl-1,2,4-triazine (7275-70-9) → 5,6-dimethyl-3-methoxy-1,2,4-triazine (28735-31-1)

Guidance literature:

In methanol; for 10h; Heating;

DOI:10.1002/jps.2600690310

Reference yield:

→ 5,6-dimethyl-3-methoxy-1,2,4-triazine (28735-31-1)

Guidance literature:

3-Methylthioverb. 4b, NaOCH3;

Reference yield: 54.0%

N-phenyl-maleimide (941-69-5) + 5,6-dimethyl-3-methoxy-1,2,4-triazine (28735-31-1) → 4-Methoxy-6,7-dimethyl-2-phenyl-pyrrolo[3,4-c]pyridine-1,3-dione (84437-50-3) + C26H23N3O5 (123346-86-1)

Guidance literature:

In xylene; at 140 ℃; for 48h;

upstream raw materials:

sodium methylate

3-methylthio-5,6-dimethyl-1,2,4-triazine

Downstream raw materials:

4-Methoxy-6,7-dimethyl-2-phenyl-pyrrolo[3,4-c]pyridine-1,3-dione

C₂₆H₂₃N₃O₅

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