C₂₆H₂₉O₅N

Base Information

Chemical Name:C₂₆H₂₉O₅N
CAS No.:951024-71-8
Molecular Formula:C₂₆H₂₉NO₅
Molecular Weight:435.52
Hs Code.:

C<sub>26</sub>H<sub>29</sub>O<sub>5</sub>N

Synonyms:C₂₆H₂₉O₅N

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Chemical Property of C₂₆H₂₉O₅N

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Technology Process of C₂₆H₂₉O₅N

There total 7 articles about C₂₆H₂₉O₅N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: C₂₃H₂₅O₅N

: 77-76-9
2,2-dimethoxy-propane

: 67-64-1
acetone

: 951024-71-8
C₂₆H₂₉O₅N

Guidance literature:: With toluene-4-sulfonic acid; at 23 ℃;
DOI:10.1021/ol701446y

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 951024-71-8
C₂₆H₂₉O₅N

Guidance literature:: Multi-step reaction with 7 steps

1.1: Br₂ / CH₂Cl₂ / 0.25 h / 0 °C

1.2: Et₃N / CH₂Cl₂ / 0.25 h

1.3: 98 percent / 72 h / 20 °C

2.1: 95 percent / pyridinium p-toluenesulfonate / 1 h / 50 °C / simultaneous removal of volatiles in vacuo

3.1: n-BuLi / hexane / -78 - -50 °C

3.2: 84 percent / hexane; tetrahydrofuran / 0.5 h / -78 °C

4.1: CeCl₃*7H₂O; NaBH₄ / ethanol / 0 °C

5.1: 6.10 g / CuSO₄*5H₂O; H₂O / methanol / 2 h / 50 °C

6.1: MgCl₂; Et₃N; TMSCl / ethyl acetate / 23 °C

6.2: trifluoroacetic acid / methanol

7.1: 82 percent / p-toluenesulfonic acid monohydrate / 23 °C

With sodium tetrahydroborate; n-butyllithium; chloro-trimethyl-silane; cerium(III) chloride; water; bromine; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; copper(II) sulfate; triethylamine; magnesium chloride; In methanol; ethanol; hexane; dichloromethane; ethyl acetate;
DOI:10.1021/ol701446y

Reference yield:

: 33603-90-6
(2Z)-2-bromo-3-phenyl-2-propenal

: 951024-71-8
C₂₆H₂₉O₅N

Guidance literature:: Multi-step reaction with 6 steps

1.1: 95 percent / pyridinium p-toluenesulfonate / 1 h / 50 °C / simultaneous removal of volatiles in vacuo

2.1: n-BuLi / hexane / -78 - -50 °C

2.2: 84 percent / hexane; tetrahydrofuran / 0.5 h / -78 °C

3.1: CeCl₃*7H₂O; NaBH₄ / ethanol / 0 °C

4.1: 6.10 g / CuSO₄*5H₂O; H₂O / methanol / 2 h / 50 °C

5.1: MgCl₂; Et₃N; TMSCl / ethyl acetate / 23 °C

5.2: trifluoroacetic acid / methanol

6.1: 82 percent / p-toluenesulfonic acid monohydrate / 23 °C

With sodium tetrahydroborate; n-butyllithium; chloro-trimethyl-silane; cerium(III) chloride; water; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; copper(II) sulfate; triethylamine; magnesium chloride; In methanol; ethanol; hexane; ethyl acetate;
DOI:10.1021/ol701446y