1-(ortho-fluorobenzyl)-3-trimethylstannyl-indene

Base Information

Chemical Name:1-(ortho-fluorobenzyl)-3-trimethylstannyl-indene
CAS No.:503445-45-2
Molecular Formula:C₁₉H₂₁FSn
Molecular Weight:387.084
Hs Code.:

Synonyms:1-(ortho-fluorobenzyl)-3-trimethylstannyl-indene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(ortho-fluorobenzyl)-3-trimethylstannyl-indene

Chemical Property:

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Technology Process of 1-(ortho-fluorobenzyl)-3-trimethylstannyl-indene

There total 1 articles about 1-(ortho-fluorobenzyl)-3-trimethylstannyl-indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1066-45-1
trimethyltin(IV)chloride

: 503445-44-1
1-(ortho-fluorobenzyl)-indene

: 503445-45-2
1-(ortho-fluorobenzyl)-3-trimethylstannyl-indene

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; byproducts: LiCl; under Ar, 1 equiv. of n-BuLi in hexane was added to ethereal soln. of indenyl-compd. at -35 °C, mixt. was allowed to warm to room temp. within 30 min, cooling to 0 °C, 1 equiv. of Me3SnCl was added in ether, 12 h; soln. was decanted, solvent was evapd., drying in vac. (80 °C, 1E-2 Torr), elem. anal.;
DOI:10.1515/znb-2002-1104

Reference yield:

: 503445-45-2
1-(ortho-fluorobenzyl)-3-trimethylstannyl-indene

: 7550-45-0
titanium tetrachloride

: C₉H₆CH₂C₆H₄FTiCl(CH₃)2

: C₉H₆CH₂C₆H₄FTi(CH₃)3

: C₉H₆CH₂C₆H₄FTiCl₂(CH₃)

: C₉H₆CH₂C₆H₄FTiCl₃

: 1066-45-1
trimethyltin(IV)chloride

Guidance literature:: In Petroleum ether; under Ar, room temp. (even at -100 °C), other products are: Me2SnCl2, MeSnCl3; detected by MS;
DOI:10.1515/znb-2002-1104