N-(2-bromo-4(1-methylethyl)phenyl)-N-ethyl-4-((4,4-ethylenedioxypiperidino)carbonyl)-6-methylpyrimidinamine

Base Information

Chemical Name:N-(2-bromo-4(1-methylethyl)phenyl)-N-ethyl-4-((4,4-ethylenedioxypiperidino)carbonyl)-6-methylpyrimidinamine
CAS No.:288625-98-9
Molecular Formula:C₂₄H₃₁BrN₄O₃
Molecular Weight:503.439
Hs Code.:

Synonyms:N-(2-bromo-4(1-methylethyl)phenyl)-N-ethyl-4-((4,4-ethylenedioxypiperidino)carbonyl)-6-methylpyrimidinamine

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Chemical Property of N-(2-bromo-4(1-methylethyl)phenyl)-N-ethyl-4-((4,4-ethylenedioxypiperidino)carbonyl)-6-methylpyrimidinamine

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Technology Process of N-(2-bromo-4(1-methylethyl)phenyl)-N-ethyl-4-((4,4-ethylenedioxypiperidino)carbonyl)-6-methylpyrimidinamine

There total 4 articles about N-(2-bromo-4(1-methylethyl)phenyl)-N-ethyl-4-((4,4-ethylenedioxypiperidino)carbonyl)-6-methylpyrimidinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 40256-14-2
4-piperidone ethylene glycol ketal

: 169880-48-2
methyl 2-((2-bromo-4-(1-methylethyl)phenyl)ethylamino)-6-methyl-4-pyrimidinecarboxylate

: 288625-98-9
N-(2-bromo-4(1-methylethyl)phenyl)-N-ethyl-4-((4,4-ethylenedioxypiperidino)carbonyl)-6-methylpyrimidinamine

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 98h; Heating / reflux;

Reference yield:

: 51605-97-1
2-bromo-4-isopropylaniline

: 288625-98-9
N-(2-bromo-4(1-methylethyl)phenyl)-N-ethyl-4-((4,4-ethylenedioxypiperidino)carbonyl)-6-methylpyrimidinamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1,4-dioxane / 20 h / Heating / reflux

2: sodium hydride / tetrahydrofuran / 24 h / Heating / reflux

3: sodium hydride / tetrahydrofuran / 98 h / 20 °C / Heating / reflux

With sodium hydride; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 89793-11-3
methyl 2-chloro-6-methylpyrimidine-4-carboxylate

: 288625-98-9
N-(2-bromo-4(1-methylethyl)phenyl)-N-ethyl-4-((4,4-ethylenedioxypiperidino)carbonyl)-6-methylpyrimidinamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1,4-dioxane / 20 h / Heating / reflux

2: sodium hydride / tetrahydrofuran / 24 h / Heating / reflux

3: sodium hydride / tetrahydrofuran / 98 h / 20 °C / Heating / reflux

With sodium hydride; In tetrahydrofuran; 1,4-dioxane;