Technology Process of (1-methylcyclohexyl)(phenyl)sulfane
There total 5 articles about (1-methylcyclohexyl)(phenyl)sulfane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3,6‐di‐tert‐butyl‐9‐mesityl‐10‐phenylacridin‐10‐ium tetrafluoroborate; cesium fluoride;
In
ethyl acetate;
at 20 ℃;
for 14h;
regioselective reaction;
Inert atmosphere;
Schlenk technique;
Irradiation;
DOI:10.1002/anie.202104595
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethyl ether; acetone / 2 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
2: 3,6‐di‐tert‐butyl‐9‐mesityl‐10‐phenylacridin‐10‐ium tetrafluoroborate; cesium fluoride / ethyl acetate / 14 h / 20 °C / Inert atmosphere; Schlenk technique; Irradiation
With
3,6‐di‐tert‐butyl‐9‐mesityl‐10‐phenylacridin‐10‐ium tetrafluoroborate; cesium fluoride;
In
diethyl ether; ethyl acetate; acetone;
DOI:10.1002/anie.202104595
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuryl dichloride / diethyl ether / 1 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
2: diethyl ether; acetone / 2 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
3: 3,6‐di‐tert‐butyl‐9‐mesityl‐10‐phenylacridin‐10‐ium tetrafluoroborate; cesium fluoride / ethyl acetate / 14 h / 20 °C / Inert atmosphere; Schlenk technique; Irradiation
With
sulfuryl dichloride; 3,6‐di‐tert‐butyl‐9‐mesityl‐10‐phenylacridin‐10‐ium tetrafluoroborate; cesium fluoride;
In
diethyl ether; ethyl acetate; acetone;
DOI:10.1002/anie.202104595
