methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-β-D-xylofuranoside]

Base Information

Chemical Name:methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-β-D-xylofuranoside]
CAS No.:551929-54-5
Molecular Formula:C₁₆H₂₂O₇S
Molecular Weight:358.412
Hs Code.:

methyl-[<i>O</i><sup>3</sup>,<i>O</i><sup>5</sup>-isopropylidene-<i>O</i><sup>2</sup>-(toluene-4-sulfonyl)-β-D-xylofuranoside]

Synonyms:methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-β-D-xylofuranoside]

Suppliers and Price of methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-β-D-xylofuranoside]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-β-D-xylofuranoside]

Chemical Property:

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Technology Process of methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-β-D-xylofuranoside]

There total 1 articles about methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-β-D-xylofuranoside] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 98-59-9
p-toluenesulfonyl chloride

: 51754-99-5
Methyl 3,5-O-Isopropylidene-β-D-xylofuranoside

: 551929-54-5
methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-β-D-xylofuranoside]

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1016/S0960-894X(03)00027-1

Reference yield:

: 551929-54-5
methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-β-D-xylofuranoside]

: 112695-36-0
methyl 2,5-di-O-benzoyl-3-fluoro-3-deoxy-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 6 steps

1: aq. AcOH

2: MeONa / methanol

3: 82 percent / KHF₂; NaF / ethane-1,2-diol / Heating

4: pyridine

5: 38 percent / 18-crown-6 / dimethylsulfoxide / Heating

With pyridine; potassium hydrogen bifluoride; 18-crown-6 ether; sodium methylate; sodium fluoride; acetic acid; In methanol; ethylene glycol; dimethyl sulfoxide;
DOI:10.1081/NCN-120022701

Reference yield:

: 551929-54-5
methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-β-D-xylofuranoside]

: 123484-12-8
((2R,3R,4S)-5-acetoxy-4-(benzoyloxy)-3-fluorotetrahydrofuran-2-yl)methyl benzoate

Guidance literature:: Multi-step reaction with 7 steps

1: aq. AcOH

2: MeONa / methanol

3: 82 percent / KHF₂; NaF / ethane-1,2-diol / Heating

4: pyridine

5: 38 percent / 18-crown-6 / dimethylsulfoxide / Heating

6: 83 percent / AcOH; H₂SO₄

With pyridine; potassium hydrogen bifluoride; 18-crown-6 ether; sulfuric acid; sodium methylate; sodium fluoride; acetic acid; In methanol; ethylene glycol; dimethyl sulfoxide;
DOI:10.1081/NCN-120022701