3-(2-furan-3-yl-ethyl)-2-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester

Base Information

• Chemical Name: 3-(2-furan-3-yl-ethyl)-2-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester
• CAS No.: 690254-66-1
• Molecular Formula: C₁₆H₂₀O₄
• Molecular Weight: 276.332

Synonyms:3-(2-furan-3-yl-ethyl)-2-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester

Chemical Property of 3-(2-furan-3-yl-ethyl)-2-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester

Chemical Property:

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Technology Process of 3-(2-furan-3-yl-ethyl)-2-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester

There total 1 articles about 3-(2-furan-3-yl-ethyl)-2-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4-carbethoxy-3-methyl-2-cyclohexen-1-one (487-51-4) + 2-(3-furyl)-1-bromoethane (98126-46-6) → 3-(2-furan-3-yl-ethyl)-2-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester (690254-66-1)

Guidance literature:

4-carbethoxy-3-methyl-2-cyclohexen-1-one; With potassium tert-butylate; In tert-butyl alcohol; at 20 ℃;

2-(3-furyl)-1-bromoethane; In tert-butyl alcohol; for 12h; Further stages.; Heating;

DOI:10.1016/j.tet.2004.01.068

Reference yield: 54.0%

3-(2-furan-3-yl-ethyl)-2-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester (690254-66-1) → 2-(2-furan-3-yl-ethyl)-3-methyl-cyclohex-2-enone (690254-59-2)

Guidance literature:

With potassium hydroxide; In ethanol; water; for 8h; Heating;

DOI:10.1016/j.tet.2004.01.068

upstream raw materials:

4-carbethoxy-3-methyl-2-cyclohexen-1-one

2-(3-furyl)-1-bromoethane

Downstream raw materials:

2-(2-furan-3-yl-ethyl)-3-methyl-cyclohex-2-enone

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