N-hydroxy-3-phenylpropanethioamide

Base Information

Chemical Name:N-hydroxy-3-phenylpropanethioamide
CAS No.:1568950-15-1
Molecular Formula:C₉H₁₁NOS
Molecular Weight:181.258
Hs Code.:

Synonyms:N-hydroxy-3-phenylpropanethioamide

Suppliers and Price of N-hydroxy-3-phenylpropanethioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-hydroxy-3-phenylpropanethioamide

Chemical Property:

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Technology Process of N-hydroxy-3-phenylpropanethioamide

There total 3 articles about N-hydroxy-3-phenylpropanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 92988-96-0
N-hydroxy(2-phenylethyl)-oximidoyl chloride

: 1568950-15-1
N-hydroxy-3-phenylpropanethioamide

Guidance literature:: With sodium sulfide; triethylamine; In diethyl ether; water; at 20 ℃; for 1h;
DOI:10.1021/jo500080x

Reference yield:

: 1197-50-8
3-phenylpropanal oxime

: 1568950-15-1
N-hydroxy-3-phenylpropanethioamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

2: sodium sulfide; triethylamine / diethyl ether; water / 1 h / 20 °C

With sodium sulfide; N-chloro-succinimide; triethylamine; In diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jo500080x

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 1568950-15-1
N-hydroxy-3-phenylpropanethioamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; hydroxylamine hydrochloride / methanol / 20 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 0.5 h / 0 °C / Darkness; Inert atmosphere

3: triethylamine; sodiumsulfide nonahydrate / water; diethyl ether / 1 h / 20 °C / Darkness; Inert atmosphere

With pyridine; N-chloro-succinimide; sodiumsulfide nonahydrate; hydroxylamine hydrochloride; triethylamine; In methanol; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1039/c6ob01003b