3-methylbut-2-en-1-yl N-((perfluorobenzoyl)oxy)-3-phenylpropanimidothioate

Base Information

Chemical Name:3-methylbut-2-en-1-yl N-((perfluorobenzoyl)oxy)-3-phenylpropanimidothioate
CAS No.:1568951-11-0
Molecular Formula:C₂₁H₁₈F₅NO₂S
Molecular Weight:443.437
Hs Code.:

Synonyms:3-methylbut-2-en-1-yl N-((perfluorobenzoyl)oxy)-3-phenylpropanimidothioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methylbut-2-en-1-yl N-((perfluorobenzoyl)oxy)-3-phenylpropanimidothioate

Chemical Property:

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Technology Process of 3-methylbut-2-en-1-yl N-((perfluorobenzoyl)oxy)-3-phenylpropanimidothioate

There total 3 articles about 3-methylbut-2-en-1-yl N-((perfluorobenzoyl)oxy)-3-phenylpropanimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

pentafluorobenzoylchloride: 2251-50-5
pentafluorobenzoylchloride

: 1568950-15-1
N-hydroxy-3-phenylpropanethioamide

: 870-63-3
prenyl bromide

: 1568951-11-0
3-methylbut-2-en-1-yl N-((perfluorobenzoyl)oxy)-3-phenylpropanimidothioate

Guidance literature:: N-hydroxy-3-phenylpropanethioamide; prenyl bromide; With tetra-(n-butyl)ammonium iodide; triethylamine; In diethyl ether; at 20 ℃;

pentafluorobenzoylchloride; With triethylamine; In diethyl ether; at 20 ℃; for 0.5h;
DOI:10.1021/jo500080x

Reference yield:

: 92988-96-0
N-hydroxy(2-phenylethyl)-oximidoyl chloride

: 1568951-11-0
3-methylbut-2-en-1-yl N-((perfluorobenzoyl)oxy)-3-phenylpropanimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium sulfide; triethylamine / diethyl ether; water / 1 h / 20 °C

2.1: triethylamine; tetra-(n-butyl)ammonium iodide / diethyl ether / 20 °C

2.2: 0.5 h / 20 °C

With sodium sulfide; tetra-(n-butyl)ammonium iodide; triethylamine; In diethyl ether; water;
DOI:10.1021/jo500080x

Reference yield:

: 1197-50-8
3-phenylpropanal oxime

: 1568951-11-0
3-methylbut-2-en-1-yl N-((perfluorobenzoyl)oxy)-3-phenylpropanimidothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

2.1: sodium sulfide; triethylamine / diethyl ether; water / 1 h / 20 °C

3.1: triethylamine; tetra-(n-butyl)ammonium iodide / diethyl ether / 20 °C

3.2: 0.5 h / 20 °C

With sodium sulfide; N-chloro-succinimide; tetra-(n-butyl)ammonium iodide; triethylamine; In diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jo500080x