(S)-N,N-dimethyl-2-phenyl-N-(pyrrolidin-2-ylmethyl)ethanaminium bromide

Base Information

Chemical Name:(S)-N,N-dimethyl-2-phenyl-N-(pyrrolidin-2-ylmethyl)ethanaminium bromide
CAS No.:1355731-10-0
Molecular Formula:Br*C₁₅H₂₅N₂
Molecular Weight:313.281
Hs Code.:

Synonyms:(S)-N,N-dimethyl-2-phenyl-N-(pyrrolidin-2-ylmethyl)ethanaminium bromide

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Chemical Property of (S)-N,N-dimethyl-2-phenyl-N-(pyrrolidin-2-ylmethyl)ethanaminium bromide

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Technology Process of (S)-N,N-dimethyl-2-phenyl-N-(pyrrolidin-2-ylmethyl)ethanaminium bromide

There total 6 articles about (S)-N,N-dimethyl-2-phenyl-N-(pyrrolidin-2-ylmethyl)ethanaminium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1355731-07-5
(S)-N-((1-(benzyloxycarbonyl)pyrrolidin-2-yl)methyl)-N,N-dimethyl-2-phenylethanaminium bromide

: 1355731-10-0
(S)-N,N-dimethyl-2-phenyl-N-(pyrrolidin-2-ylmethyl)ethanaminium bromide

Guidance literature:: With 10% Pd/C; hydrogen; In ethanol; at 20 ℃; for 24h; under 760.051 Torr;
DOI:10.1007/s11164-011-0480-y

Reference yield:

: 123803-29-2
(S)-benzyl 2-((methylsulfonyloxy)methyl)pyrrolidine-1-carboxylate

: 1355731-10-0
(S)-N,N-dimethyl-2-phenyl-N-(pyrrolidin-2-ylmethyl)ethanaminium bromide

Guidance literature:: Multi-step reaction with 4 steps

1: lithium bromide / tetrahydrofuran / 67 °C

2: water; methanol / 55 °C

3: acetonitrile / 85 °C

4: 10% Pd/C; hydrogen / ethanol / 24 h / 20 °C / 760.05 Torr

With 10% Pd/C; hydrogen; lithium bromide; In tetrahydrofuran; methanol; ethanol; water; acetonitrile;
DOI:10.1007/s11164-011-0480-y

Reference yield:

: (S)-benzyl 2-(bromomethyl)pyrrolidine-1-carboxylate

: 1355731-10-0
(S)-N,N-dimethyl-2-phenyl-N-(pyrrolidin-2-ylmethyl)ethanaminium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: water; methanol / 55 °C

2: acetonitrile / 85 °C

3: 10% Pd/C; hydrogen / ethanol / 24 h / 20 °C / 760.05 Torr

With 10% Pd/C; hydrogen; In methanol; ethanol; water; acetonitrile;
DOI:10.1007/s11164-011-0480-y