(S)-N-((1-(benzyloxycarbonyl)pyrrolidin-2-yl)methyl)-N,N-dimethyl-2-phenylethanaminium bromide

Base Information

Chemical Name:(S)-N-((1-(benzyloxycarbonyl)pyrrolidin-2-yl)methyl)-N,N-dimethyl-2-phenylethanaminium bromide
CAS No.:1355731-07-5
Molecular Formula:Br*C₂₃H₃₁N₂O₂
Molecular Weight:447.415
Hs Code.:

Synonyms:(S)-N-((1-(benzyloxycarbonyl)pyrrolidin-2-yl)methyl)-N,N-dimethyl-2-phenylethanaminium bromide

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Chemical Property of (S)-N-((1-(benzyloxycarbonyl)pyrrolidin-2-yl)methyl)-N,N-dimethyl-2-phenylethanaminium bromide

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Technology Process of (S)-N-((1-(benzyloxycarbonyl)pyrrolidin-2-yl)methyl)-N,N-dimethyl-2-phenylethanaminium bromide

There total 6 articles about (S)-N-((1-(benzyloxycarbonyl)pyrrolidin-2-yl)methyl)-N,N-dimethyl-2-phenylethanaminium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1316160-31-2
(S)-benzyl 2-((dimethylamino) methyl)pyrrolidine-1-carboxylate

: 103-63-9
1-phenyl-2-bromoethane

: 1355731-07-5
(S)-N-((1-(benzyloxycarbonyl)pyrrolidin-2-yl)methyl)-N,N-dimethyl-2-phenylethanaminium bromide

Guidance literature:: In acetonitrile; at 85 ℃;
DOI:10.1007/s11164-011-0480-y

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1355731-07-5
(S)-N-((1-(benzyloxycarbonyl)pyrrolidin-2-yl)methyl)-N,N-dimethyl-2-phenylethanaminium bromide

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: triethylamine / dichloromethane / 0 - 20 °C

3: lithium bromide / tetrahydrofuran / 67 °C

4: water; methanol / 55 °C

5: acetonitrile / 85 °C

With triethylamine; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1007/s11164-011-0480-y

Reference yield:

: 123803-29-2
(S)-benzyl 2-((methylsulfonyloxy)methyl)pyrrolidine-1-carboxylate

: 1355731-07-5
(S)-N-((1-(benzyloxycarbonyl)pyrrolidin-2-yl)methyl)-N,N-dimethyl-2-phenylethanaminium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium bromide / tetrahydrofuran / 67 °C

2: water; methanol / 55 °C

3: acetonitrile / 85 °C

With lithium bromide; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1007/s11164-011-0480-y