5-O-acetyl-2-O-benzyl-3-O-t-butyldimethylsilyl-6-deoxytalofuranolactone

Base Information

Chemical Name:5-O-acetyl-2-O-benzyl-3-O-t-butyldimethylsilyl-6-deoxytalofuranolactone
CAS No.:151896-45-6
Molecular Formula:C₂₁H₃₂O₆Si
Molecular Weight:408.567
Hs Code.:

Synonyms:5-O-acetyl-2-O-benzyl-3-O-t-butyldimethylsilyl-6-deoxytalofuranolactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-O-acetyl-2-O-benzyl-3-O-t-butyldimethylsilyl-6-deoxytalofuranolactone

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Technology Process of 5-O-acetyl-2-O-benzyl-3-O-t-butyldimethylsilyl-6-deoxytalofuranolactone

There total 4 articles about 5-O-acetyl-2-O-benzyl-3-O-t-butyldimethylsilyl-6-deoxytalofuranolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 75-36-5
acetyl chloride

: 151896-34-3
2-O-benzyl-3-O-t-butyldimethylsilyl-6-deoxytalofuranolactone

: 151896-45-6
5-O-acetyl-2-O-benzyl-3-O-t-butyldimethylsilyl-6-deoxytalofuranolactone

Guidance literature:: With pyridine; In dichloromethane; for 4h; Ambient temperature;

Reference yield:

: 129320-37-2
S-ethyl (2R,3R,4E)-2-benzyloxy-3-hydroxy-4-hexenethioate

: 151896-45-6
5-O-acetyl-2-O-benzyl-3-O-t-butyldimethylsilyl-6-deoxytalofuranolactone

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 8.5 h / Ambient temperature

2: 72 percent / N-methylmorpholine N-oxide, OsO₄ / acetone; H₂O / 1.) 0 deg C, 17 h, 2.) RT, 30 h

3: 97 percent / pyridine / CH₂Cl₂ / 4 h / Ambient temperature

With pyridine; 1H-imidazole; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 151896-45-6
5-O-acetyl-2-O-benzyl-3-O-t-butyldimethylsilyl-6-deoxytalofuranolactone

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 8.5 h / Ambient temperature

2: 72 percent / N-methylmorpholine N-oxide, OsO₄ / acetone; H₂O / 1.) 0 deg C, 17 h, 2.) RT, 30 h

3: 97 percent / pyridine / CH₂Cl₂ / 4 h / Ambient temperature

With pyridine; 1H-imidazole; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In dichloromethane; water; N,N-dimethyl-formamide; acetone;