1-(3-fluoro-4-methoxyphenyl)-2-(4-aminosulphonylphenyl)-ethan-1-one oxime

Base Information

Chemical Name:1-(3-fluoro-4-methoxyphenyl)-2-(4-aminosulphonylphenyl)-ethan-1-one oxime
CAS No.:181697-23-4
Molecular Formula:C₁₅H₁₅FN₂O₄S
Molecular Weight:338.36
Hs Code.:

Synonyms:1-(3-fluoro-4-methoxyphenyl)-2-(4-aminosulphonylphenyl)-ethan-1-one oxime

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Chemical Property of 1-(3-fluoro-4-methoxyphenyl)-2-(4-aminosulphonylphenyl)-ethan-1-one oxime

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Technology Process of 1-(3-fluoro-4-methoxyphenyl)-2-(4-aminosulphonylphenyl)-ethan-1-one oxime

There total 4 articles about 1-(3-fluoro-4-methoxyphenyl)-2-(4-aminosulphonylphenyl)-ethan-1-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 177561-49-8
1-(3-fluoro-4-methoxyphenyl)-2-(4-aminosulphonylphenyl)-ethan-1-one

: 181697-23-4
1-(3-fluoro-4-methoxyphenyl)-2-(4-aminosulphonylphenyl)-ethan-1-one oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; at 75 ℃; for 2h; Heating / reflux;

Reference yield:

: 4-[2-(3-fluoro-4-methoxy-phenyl)-2-oxo-ethyl]-benzenesulfonyl chloride

: 181697-23-4
1-(3-fluoro-4-methoxyphenyl)-2-(4-aminosulphonylphenyl)-ethan-1-one oxime

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / dichloromethane; water / 16 h

2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 2 h / 75 °C / Heating / reflux

With hydroxylamine hydrochloride; ammonia; sodium acetate; In ethanol; dichloromethane; water;

Reference yield:

: 321-28-8
1-fluoro-2-methoxybenzene

: 181697-23-4
1-(3-fluoro-4-methoxyphenyl)-2-(4-aminosulphonylphenyl)-ethan-1-one oxime

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride / dichloromethane / 1 h / 2 °C

2: chlorosulfonic acid / 3 h / 0 - 20 °C

3: ammonia / dichloromethane; water / 16 h

4: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 2 h / 75 °C / Heating / reflux

With chlorosulfonic acid; aluminum (III) chloride; hydroxylamine hydrochloride; ammonia; sodium acetate; In ethanol; dichloromethane; water;